(μ-((R(p),R(p))-bis[2-(diphenylphospino)ferrocen-1-yl]methane-P,P))hexahydrodiboron

Base Information

Chemical Name:(μ-((R(p),R(p))-bis[2-(diphenylphospino)ferrocen-1-yl]methane-P,P))hexahydrodiboron
CAS No.:914249-83-5
Molecular Formula:C₄₅H₄₄B₂Fe₂P₂
Molecular Weight:780.108
Hs Code.:

Synonyms:(μ-((R(p),R(p))-bis[2-(diphenylphospino)ferrocen-1-yl]methane-P,P))hexahydrodiboron

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Chemical Property of (μ-((R(p),R(p))-bis[2-(diphenylphospino)ferrocen-1-yl]methane-P,P))hexahydrodiboron

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Technology Process of (μ-((R(p),R(p))-bis[2-(diphenylphospino)ferrocen-1-yl]methane-P,P))hexahydrodiboron

There total 1 articles about (μ-((R(p),R(p))-bis[2-(diphenylphospino)ferrocen-1-yl]methane-P,P))hexahydrodiboron which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 14044-65-6
borane-THF

: 914249-86-8
(R(p),R(p))-bis[2-(tributylstannyl)ferrocen-1-yl]methane

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 914249-83-5
(μ-((R(p),R(p))-bis[2-(diphenylphospino)ferrocen-1-yl]methane-P,P))hexahydrodiboron

Guidance literature:: With (CH₃)3CLi; In tetrahydrofuran; hexane; (Ar); (CH3)3CLi in hexane added dropwise to a soln. of Fe complex in THFat 0°C, stirred at 0°C for 10 min, (C6H5)2PCl added, stir red for 30 min at 0°C, stirred at room temp., BH3 in THF added, stirred for 16 h at room temp.; quenched with aq. NaHCO3, extd. (Et2O), washed (H2O, brine), dried (MgSO4), concd. (vac.), chromd. (petroleum ether/Et2O/Et3N);
DOI:10.1002/hlca.200690173

Reference yield: 98.0%

: 914249-83-5
(μ-((R(p),R(p))-bis[2-(diphenylphospino)ferrocen-1-yl]methane-P,P))hexahydrodiboron

: 914249-81-3,914249-89-1
(R(p),R(p))-bis[2-(diphenylphospino)ferrocen-1-yl]methane

Guidance literature:: With (C₂H₅)2NH; In diethylamine; (Ar); a soln. of Fe complex stirred for 4 h at room temp.; evapd. (vac.), chromd. (petroleum ether/Et2O/Et3N); elem. anal.;
DOI:10.1002/hlca.200690173