diphenyllead bis(4-chlorobenzenecarboselenoate)

Base Information

• Chemical Name: diphenyllead bis(4-chlorobenzenecarboselenoate)
• CAS No.: 128816-60-4
• Molecular Formula: C₂₆H₁₈Cl₂O₂PbSe₂
• Molecular Weight: 798.454
• Mol file: 128816-60-4.mol

Synonyms:diphenyllead bis(4-chlorobenzenecarboselenoate)

Chemical Property of diphenyllead bis(4-chlorobenzenecarboselenoate)

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of diphenyllead bis(4-chlorobenzenecarboselenoate)

There total 1 articles about diphenyllead bis(4-chlorobenzenecarboselenoate) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

diphenyllead(IV) dichloride (2117-69-3) + potassium 4-chlorobenzenecarboselenoate → diphenyllead bis(4-chlorobenzenecarboselenoate) (128816-60-4)

Guidance literature:

In diethyl ether; byproducts: KCl; addn. of Ph2PbCl2 to a suspn. of K-selenocarboxylate in ether, stirring at 20°C for 1 h (under Ar); filtn. of KCl-ppt., evapn. of the solvent in vacuo, recrystn. from ether/hexane, elem. anal.;

DOI:10.1016/0022-328X(90)80004-J

Reference yield: 80.0%

Phenylselenyl bromide (34837-55-3) + diphenyllead bis(4-chlorobenzenecarboselenoate) (128816-60-4) → Se(Se)-phenyl 4-chlorodiselenoperbenzoate (59502-03-3)

Guidance literature:

In dichloromethane; at 20 ℃; for 2h;

DOI:10.1016/0022-328X(90)80004-J

upstream raw materials:

diphenyllead(IV) dichloride

Downstream raw materials:

Se(Se)-phenyl 4-chlorodiselenoperbenzoate