Benzyl -β-D-ribo-decofuranosid>uronate

Base Information

Chemical Name:Benzyl -β-D-ribo-decofuranosid>uronate
CAS No.:160451-23-0
Molecular Formula:C₂₈H₃₇NO₈S
Molecular Weight:547.67
Hs Code.:

Benzyl <methyl 2,3-O-(isopropylidene)-5,6,7,8,9-pentadeoxy-9(S)-<(p-toluenesulfonyl)amino>-β-D-ribo-decofuranosid>uronate

Synonyms:Benzyl -β-D-ribo-decofuranosid>uronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl -β-D-ribo-decofuranosid>uronate

Chemical Property:

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Technology Process of Benzyl -β-D-ribo-decofuranosid>uronate

There total 10 articles about Benzyl -β-D-ribo-decofuranosid>uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: Benzyl -6-(p-toluenesulfonylhydrazono)-β-D-ribo-decofuranosid>uronate

: 160451-23-0
Benzyl -β-D-ribo-decofuranosid>uronate

Guidance literature:: With benzo[1,3,2]dioxaborole; In tetrahydrofuran; chloroform; at 0 ℃; for 24h;
DOI:10.1021/jo00094a033

Reference yield:

: 33985-40-9
(3aR,4S,6R,6aR)-tetrahydro-6-methoxy-2,2-dimethylfuro-[3,4-d][1,3]dioxole-4-carbaldehyde

: 160451-23-0
Benzyl -β-D-ribo-decofuranosid>uronate

Guidance literature:: Multi-step reaction with 6 steps

1: F(-)

2: dehydratation

3: reduction

4: ceric ammonium nitrate

5: 94 percent / oxalic acid / ethanol / 24 h / 22 °C

6: 50 percent / catecholborane / tetrahydrofuran; CHCl₃ / 24 h / 0 °C

With ammonium cerium(IV) nitrate; oxalic acid; benzo[1,3,2]dioxaborole; fluoride; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jo00094a033

Reference yield:

: 2978-10-1
O-benzyl-N,N'-diisopropylisourea

: 160451-23-0
Benzyl -β-D-ribo-decofuranosid>uronate

Guidance literature:: Multi-step reaction with 7 steps

2: F(-)

3: dehydratation

4: reduction

5: ceric ammonium nitrate

6: 94 percent / oxalic acid / ethanol / 24 h / 22 °C

7: 50 percent / catecholborane / tetrahydrofuran; CHCl₃ / 24 h / 0 °C

With ammonium cerium(IV) nitrate; oxalic acid; benzo[1,3,2]dioxaborole; fluoride; In tetrahydrofuran; ethanol; chloroform;
DOI:10.1021/jo00094a033