1,4-dibromo-2,3-butanediol

Base Information

• Chemical Name: 1,4-dibromo-2,3-butanediol
• CAS No.: 19396-65-7
• Molecular Weight: 0
• Mol file: 19396-65-7.mol

Synonyms:CL012

Chemical Property of 1,4-dibromo-2,3-butanediol

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1,4-dibromo-2,3-butanediol

There total 2 articles about 1,4-dibromo-2,3-butanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Mo2O2(μ-O,S)[S2CN(n-Bu)2]2 (67368-85-8) + phosphorous (V) sulfide → Mo2O2(μ-S2)[S2CN(n-Bu)2]2 (60428-79-7,19396-65-7) + Mo2OS(μ-S2)[S2CN(n-Bu)2]2 (67368-86-9,69779-87-9) + Mo2S4{(C4H9)2NCS2}2

Guidance literature:

In not given; chromy. (HPLC: silica gel, hexane-ethanol; octadecylsilane, water-methanol); elem. anal.;

Reference yield:

sodium hydrogen sulfide + di-n-butyldithiocarbamate(1-) (22296-18-0) + molybdenum(VI) oxide → Mo2O2(μ-S2)[S2CN(n-Bu)2]2 (60428-79-7,19396-65-7) + Mo2OS(μ-S2)[S2CN(n-Bu)2]2 (67368-86-9,69779-87-9)

Guidance literature:

In not given; chromy. (HPLC: silica gel, hexane-ethanol; octadecylsilane, water-methanol); elem. anal.;

upstream raw materials:

Mo2O2(μ-O,S)[S2CN(n-Bu)2]2

di-n-butyldithiocarbamate^(1-)