4-methoxyphenyl 2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside

Base Information

• Chemical Name: 4-methoxyphenyl 2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside
• CAS No.: 1096154-21-0
• Molecular Formula: C₄₇H₄₄O₁₄
• Molecular Weight: 832.858

Synonyms:4-methoxyphenyl 2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside

Chemical Property of 4-methoxyphenyl 2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside

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Technology Process of 4-methoxyphenyl 2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside

There total 1 articles about 4-methoxyphenyl 2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

4-methoxyphenyl 3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside (1096154-20-9) → 4-methoxyphenyl 2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside (1096154-21-0)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; triethylamine; triphenylphosphine; In tetrahydrofuran; at 25 ℃;

DOI:10.1016/j.carres.2008.09.010

Reference yield: 76.0%

4-methoxyphenyl 2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside (1096154-21-0) + 2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl trichloroacetimidate (502615-41-0) → 4-methoxyphenyl 2,3,4-tri-O-benzoyl-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside (1096154-23-2)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at -10 ℃; for 2h;

DOI:10.1016/j.carres.2008.09.010

upstream raw materials:

4-methoxyphenyl 3-O-allyloxycarbonyl-2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside

Downstream raw materials:

4-methoxyphenyl 2,3,4-tri-O-benzoyl-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-L-rhamnopyranosyl-(1->3)-2,4-di-O-benzoyl-α-L-rhamnopyranosyl-(1->2)-3,4-di-O-benzoyl-6-deoxy-L-talopyranoside

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