1-(2-Aminoethoxy)-2-methylcyclohexane

Base Information

Chemical Name:1-(2-Aminoethoxy)-2-methylcyclohexane
CAS No.:19785-67-2
Molecular Formula:C₉H₁₉NO
Molecular Weight:157.256
Hs Code.:
European Community (EC) Number:973-335-1

Synonyms:1-(2-aminoethoxy)-2-methylcyclohexane;2-[(2-methylcyclohexyl)oxy]ethanamine;19785-67-2;2-(2-methylcyclohexyl)oxyethanamine;AKOS000152739;AKOS022478008;2-[(2-methylcyclohexyl)oxy]ethan-1-amine;EN300-41211;G27454;Z285179000

Suppliers and Price of 1-(2-Aminoethoxy)-2-methylcyclohexane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 1-(2-Aminoethoxy)-2-methylcyclohexane

Chemical Property:

XLogP3:1.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:157.146664230
Heavy Atom Count:11
Complexity:106

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1CCCCC1OCCN

Technology Process of 1-(2-Aminoethoxy)-2-methylcyclohexane

There total 4 articles about 1-(2-Aminoethoxy)-2-methylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 19785-66-1
2-((2-methylcyclohexyl)oxy)acetamide

: 19785-67-2
2-((2-methylcyclohexyl)oxy)ethan-1-amine

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 22h; Inert atmosphere; Reflux;
DOI:10.1002/anie.201902513

Reference yield:

: 519050-83-0
(2-methylcyclohexyl)oxyacetic acid

: 19785-67-2
2-((2-methylcyclohexyl)oxy)ethan-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1: SOCl₂

2: aq. NH₃

3: LiAlH₄

With ammonium hydroxide; lithium aluminium tetrahydride; thionyl chloride;

Reference yield:

: 583-59-5
2-Methylcyclohexanol

: 19785-67-2
2-((2-methylcyclohexyl)oxy)ethan-1-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium / tetrahydrofuran / 16 h / Inert atmosphere; Reflux

1.2: 6 h / Inert atmosphere; Reflux

2.1: thionyl chloride / 2 h / 50 °C

2.2: 15 h / 20 °C / Cooling with ice

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 22 h / Inert atmosphere; Reflux

With lithium aluminium tetrahydride; thionyl chloride; lithium; In tetrahydrofuran;
DOI:10.1002/anie.201902513