4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene

Base Information

• Chemical Name: 4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene
• CAS No.: 205643-55-6
• Molecular Formula: C₂₄H₂₄N₂O
• Molecular Weight: 356.467

Synonyms:4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene

Chemical Property of 4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene

There total 3 articles about 4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-cycloheptatrienylidene-4-methyl-aniline (949-68-8) + mesitylenecarbonitrile oxide (2904-57-6) → 4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene (205643-58-9) + 4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene (205643-55-6) + p-tolyl-[3-(2,4,6-trimethyl-phenyl)-3aH-cyclohepta[d]isoxazol-4-yl]-amine + p-tolyl-[3-(2,4,6-trimethyl-phenyl)-8aH-cyclohepta[d]isoxazol-4-yl]-amine

Guidance literature:

In cyclohexane; at 35 ℃; for 60h; Yield given; Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;

DOI:10.3987/com-97-s(n)76

Reference yield:

N-cycloheptatrienylidene-4-methyl-aniline (949-68-8) + mesitylenecarbonitrile oxide (2904-57-6) → 4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene (205643-58-9) + 4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene (205643-55-6)

Guidance literature:

In methanol; for 1h; Yield given; Yields of byproduct given. Title compound not separated from byproducts; Ambient temperature;

DOI:10.3987/com-97-s(n)76

Reference yield:

4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene (205643-58-9) → 4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-4,9a-dihydro-1-oxa-2,4-diaza-benzocycloheptene (205643-55-6)

Guidance literature:

In benzene-d6; at 20 ℃; Product distribution; equilibrium reaction; other deuteriated solvents;

DOI:10.3987/com-97-s(n)76

upstream raw materials:

N-cycloheptatrienylidene-4-methyl-aniline

mesitylenecarbonitrile oxide

4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene

Downstream raw materials:

cyanomesitylene

p-Tolylisocyanate

4-p-tolyl-3-(2,4,6-trimethyl-phenyl)-1-oxa-2,4-diaza-spiro[4.6]undeca-2,6,8,10-tetraene

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