4-cetyloxy-3-methoxybenzophenone-(E)-3-methoxycarbonylphenylsulfohydrazone

Base Information

Chemical Name:4-cetyloxy-3-methoxybenzophenone-(E)-3-methoxycarbonylphenylsulfohydrazone
CAS No.:926292-01-5
Molecular Formula:C₃₈H₅₂N₂O₆S
Molecular Weight:664.907
Hs Code.:

Synonyms:4-cetyloxy-3-methoxybenzophenone-(E)-3-methoxycarbonylphenylsulfohydrazone

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Chemical Property of 4-cetyloxy-3-methoxybenzophenone-(E)-3-methoxycarbonylphenylsulfohydrazone

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Technology Process of 4-cetyloxy-3-methoxybenzophenone-(E)-3-methoxycarbonylphenylsulfohydrazone

There total 5 articles about 4-cetyloxy-3-methoxybenzophenone-(E)-3-methoxycarbonylphenylsulfohydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 926291-90-9
3-methoxycarbonylbenzenesulfohydrazide

: 926291-91-0
4-cetyloxy-3-methoxybenzophenone

: 926292-02-6
4-cetyloxy-3-methoxybenzophenone-(Z)-3-methoxycarbonylphenylsulfohydrazone

: 926292-01-5
4-cetyloxy-3-methoxybenzophenone-(E)-3-methoxycarbonylphenylsulfohydrazone

Guidance literature:: In methanol; for 18h; Heating;
DOI:10.1021/jm060834d

Reference yield:

: 51439-89-5
(4-hydroxy-3-methoxyphenyl)(phenyl)methanone

: 926292-01-5
4-cetyloxy-3-methoxybenzophenone-(E)-3-methoxycarbonylphenylsulfohydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / Na₂CO₃ / dimethylformamide / 2 h / 80 °C

2: 32 percent / methanol / 18 h / Heating

With sodium carbonate; In methanol; N,N-dimethyl-formamide;
DOI:10.1021/jm060834d

Reference yield:

: 4025-64-3
3-Carboxybenzenesulfonyl chloride

: 926292-01-5
4-cetyloxy-3-methoxybenzophenone-(E)-3-methoxycarbonylphenylsulfohydrazone

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 2 h / Heating

1.2: 0.25 h

2.1: 367 mg / hydrazine hydrate / ethanol; CHCl₃ / 0.5 h / 0 °C

3.1: 32 percent / methanol / 18 h / Heating

With thionyl chloride; hydrazine hydrate; In methanol; ethanol; chloroform;
DOI:10.1021/jm060834d