4-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-5-methoxycyclohexa-1,3-dienecarboxylic acid

Base Information

Chemical Name:4-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-5-methoxycyclohexa-1,3-dienecarboxylic acid
CAS No.:1609477-34-0
Molecular Formula:C₂₅H₃₂O₇
Molecular Weight:444.525
Hs Code.:

Synonyms:4-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-5-methoxycyclohexa-1,3-dienecarboxylic acid

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Chemical Property of 4-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-5-methoxycyclohexa-1,3-dienecarboxylic acid

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Technology Process of 4-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-5-methoxycyclohexa-1,3-dienecarboxylic acid

There total 7 articles about 4-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-5-methoxycyclohexa-1,3-dienecarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609477-88-4
C₂₆H₃₄O₇

: 1609477-34-0
4-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-5-methoxycyclohexa-1,3-dienecarboxylic acid

Guidance literature:: C₂₆H₃₄O₇; With potassium hydroxide; In 1,4-dioxane; water; for 12h; Inert atmosphere;

With hydrogenchloride; In 1,4-dioxane; dichloromethane; water;
DOI:10.1021/jm5000563

Reference yield:

: 3943-74-6
4-hydroxy-3-methoxybenzoic acid methyl ester

: 1609477-34-0
4-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-5-methoxycyclohexa-1,3-dienecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetonitrile / 6 h / 85 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetonitrile / 0.25 h / 160 °C / Inert atmosphere; Microwave irradiation

3: potassium hydroxide / 1,4-dioxane; water / 12 h / Inert atmosphere

With potassium carbonate; potassium iodide; potassium hydroxide; In 1,4-dioxane; water; acetonitrile;
DOI:10.1021/jm5000563

Reference yield:

: 7065-46-5
3,3-dimethylbutanoic acid chloride

: 1609477-34-0
4-(4-(4-(3,3-dimethylbutanoyl)-3-hydroxy-2-methylphenoxy)-butoxy)-5-methoxycyclohexa-1,3-dienecarboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: aluminum (III) chloride / dichloromethane / 12 h / 0 - 20 °C / Inert atmosphere

2: potassium carbonate; potassium iodide / acetonitrile / 0.25 h / 160 °C / Inert atmosphere; Microwave irradiation

3: potassium hydroxide / 1,4-dioxane; water / 12 h / Inert atmosphere

With aluminum (III) chloride; potassium carbonate; potassium iodide; potassium hydroxide; In 1,4-dioxane; dichloromethane; water; acetonitrile; 1: |Friedel-Crafts Acylation;
DOI:10.1021/jm5000563