Trifluoro-methanesulfonate((2S,3R)-3-benzenesulfonylamino-3-carboxy-2-hydroxy-propyl)-benzyl-methyl-sulfonium;

Base Information

Chemical Name:Trifluoro-methanesulfonate((2S,3R)-3-benzenesulfonylamino-3-carboxy-2-hydroxy-propyl)-benzyl-methyl-sulfonium;
CAS No.:119593-62-3
Molecular Formula:CF₃O₃S*C₁₈H₂₂NO₅S₂
Molecular Weight:545.579
Hs Code.:

Synonyms:Trifluoro-methanesulfonate((2S,3R)-3-benzenesulfonylamino-3-carboxy-2-hydroxy-propyl)-benzyl-methyl-sulfonium;

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Chemical Property of Trifluoro-methanesulfonate((2S,3R)-3-benzenesulfonylamino-3-carboxy-2-hydroxy-propyl)-benzyl-methyl-sulfonium;

Chemical Property:

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Technology Process of Trifluoro-methanesulfonate((2S,3R)-3-benzenesulfonylamino-3-carboxy-2-hydroxy-propyl)-benzyl-methyl-sulfonium;

There total 10 articles about Trifluoro-methanesulfonate((2S,3R)-3-benzenesulfonylamino-3-carboxy-2-hydroxy-propyl)-benzyl-methyl-sulfonium; which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 119593-60-1
benzyl<(2S,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

: 119593-62-3
Trifluoro-methanesulfonate((2S,3R)-3-benzenesulfonylamino-3-carboxy-2-hydroxy-propyl)-benzyl-methyl-sulfonium;

Guidance literature:: With oxygen; platinum(IV) oxide; In water; isopropyl alcohol; at 60 ℃; for 18h;
DOI:10.1021/jo00269a023

Reference yield: 87.0%

: 119717-05-4
benzyl<(2R,3S)-2,4-dihydroxy-3-<(phenylsulfonyl)amino>-1-butyl>methylsulfonium triflate

: 119593-62-3
Trifluoro-methanesulfonate((2R,3R)-3-benzenesulfonylamino-3-carboxy-2-hydroxy-propyl)-benzyl-methyl-sulfonium;

Guidance literature:: With oxygen; platinum(IV) oxide; In water; isopropyl alcohol; at 60 ℃; for 18h;
DOI:10.1021/jo00269a023

Reference yield:

: 17674-16-7
benzyl triflate

: 119593-62-3
Trifluoro-methanesulfonate((2S,3R)-3-benzenesulfonylamino-3-carboxy-2-hydroxy-propyl)-benzyl-methyl-sulfonium;

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / Hunig's base / CH₂Cl₂ / 0.5 h / -45 °C

2: 87 percent / O₂ / PtO₂ / H₂O; propan-2-ol / 18 h / 60 °C

With oxygen; N-ethyl-N,N-diisopropylamine; platinum(IV) oxide; In dichloromethane; water; isopropyl alcohol;
DOI:10.1021/jo00269a023