DICHLOROMETHYLTRIMETHYLGERMANE

Base Information

• Chemical Name: DICHLOROMETHYLTRIMETHYLGERMANE
• CAS No.: 19272-94-7
• Molecular Formula: C₄H₁₀Cl₂Ge
• Molecular Weight: 201.619
• Hs Code.: 2931900090
• Mol file: 19272-94-7.mol

Synonyms:DICHLOROMETHYLTRIMETHYLGERMANE

Chemical Property of DICHLOROMETHYLTRIMETHYLGERMANE

Chemical Property:

• Vapor Pressure: 7.26mmHg at 25°C
• Refractive Index: 1.4653
• Boiling Point: 149-50°C
• Flash Point: 33°C
• PSA: 0.00000
• Density: 1,334 g/cm3
• LogP: 3.08740

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DICHLOROMETHYLTRIMETHYLGERMANE

There total 1 articles about DICHLOROMETHYLTRIMETHYLGERMANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

trimethylbromogermane (1066-37-1) → Trimethyl-dichlormethyl-german (19272-94-7)

Guidance literature:

With chloroform; ammonium chloride; In tetrahydrofuran; soln. CHCl3/THF cooled to -90°C, addn. i-PrMgCl/THF over 15 min at -80°C, addn. Me3GeBr/THF (same temp.), mixt. stirred (-80°C, 0.5h), allowed to warm to room temp.; hydrolysed with satd. NH4Cl, organic layer separated, dried (Na2SO4), distilled, elem. anal.;

DOI:10.1016/0022-328X(86)84029-3

upstream raw materials:

trimethylbromogermane