(2R,3R,4R)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester

Base Information

Chemical Name:(2R,3R,4R)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester
CAS No.:1059067-72-9
Molecular Formula:C₄₄H₆₃NO₈Si
Molecular Weight:762.072
Hs Code.:

(2R,3R,4R)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester

Synonyms:(2R,3R,4R)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester

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Chemical Property of (2R,3R,4R)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester

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Technology Process of (2R,3R,4R)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester

There total 2 articles about (2R,3R,4R)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1059067-67-2
(2S,3E)-2-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)-2-benzyloxymethylhex-3-enoic acid 8-phenylmenthyl ester

: 1059067-72-9
(2R,3R,4R)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester

Guidance literature:: With potassium osmate(VI) dihydrate; methanesulfonamide; water; potassium carbonate; 10,11-dihydroquinidine p-chlorobenzoate; potassium hexacyanoferrate(III); In tert-butyl alcohol; at 20 ℃; for 36h; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/ol801709c

Reference yield:

: 1059067-67-2
(2S,3E)-2-benzyloxycarbonylamino-6-(tert-butyldimethylsilanyloxy)-2-benzyloxymethylhex-3-enoic acid 8-phenylmenthyl ester

: (2R,3S,4S)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester

: 1059067-72-9
(2R,3R,4R)-2-benzyloxycarbonylamino-2-benzyloxymethyl-6-(tertbutyldimethylsilanyloxy)-3,4-dihydroxyhexanoic acid 8-phenylmenthyl ester

Guidance literature:: With potassium osmate(VI) dihydrate; water; 4-methylmorpholine N-oxide; In acetone; for 120h; optical yield given as %de; diastereoselective reaction;
DOI:10.1021/ol801709c