C₁₄H₁₂F₆N₄O₂

Base Information

Chemical Name:C₁₄H₁₂F₆N₄O₂
CAS No.:1400917-15-8
Molecular Formula:C₁₄H₁₂F₆N₄O₂
Molecular Weight:382.265
Hs Code.:

C<sub>14</sub>H<sub>12</sub>F<sub>6</sub>N<sub>4</sub>O<sub>2</sub>

Synonyms:C₁₄H₁₂F₆N₄O₂

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Chemical Property of C₁₄H₁₂F₆N₄O₂

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Technology Process of C₁₄H₁₂F₆N₄O₂

There total 6 articles about C₁₄H₁₂F₆N₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1400917-14-7
C₁₉H₂₀F₆N₄O₄

: 1400917-15-8
C₁₄H₁₂F₆N₄O₂

Guidance literature:: With water; trifluoroacetic acid; In dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2012.07.069

Reference yield:

: 1400916-92-8
C₁₇H₁₇F₃N₂O₄

: 1400917-15-8
C₁₄H₁₂F₆N₄O₂

Guidance literature:: Multi-step reaction with 5 steps

1: hydrogen; 10% Pd/C / ethyl acetate / 6 h / 20 °C

2: triethylamine; diphenyl phosphoryl azide / 8 h / 83 °C

3: lithium hydroxide; water / tetrahydrofuran / 72 h / 20 °C

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 80 °C

5: water; trifluoroacetic acid / dichloromethane / 20 °C

With diphenyl phosphoryl azide; 10% Pd/C; water; hydrogen; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; 2: |Curtius Rearrangement;
DOI:10.1016/j.tet.2012.07.069

Reference yield:

: 1400917-09-0
C₁₄H₂₀F₃N₃O₄

: 1400917-15-8
C₁₄H₁₂F₆N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1: lithium hydroxide; water / tetrahydrofuran / 72 h / 20 °C

2: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 80 °C

3: water; trifluoroacetic acid / dichloromethane / 20 °C

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; lithium hydroxide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.tet.2012.07.069