(2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran

Base Information

Chemical Name:(2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran
CAS No.:1443117-65-4
Molecular Formula:C₂₀H₂₄O₃
Molecular Weight:312.409
Hs Code.:

Synonyms:(2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran

Suppliers and Price of (2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran

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Technology Process of (2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran

There total 7 articles about (2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1443117-67-6
(2S,3S,4S,5R)-ethyl 2-benzyl-4-hydroxymethyl-3-methyl-5-phenyltetrahydrofuran-2-carboxylate

: 1443117-65-4
(2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 2h;
DOI:10.1021/jo400858u

Reference yield: 90.0%

: 1443117-68-7
(2S,3S,4S,5R)-yl 2-benzyl-4-hydroxymethyl-3-methyl-5-phenyltetrahydrofuran-2-carboxylate

: 1443117-65-4
(2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran

Guidance literature:: With lithium aluminium tetrahydride; In diethyl ether; at 20 ℃; for 2h;
DOI:10.1021/jo400858u

Reference yield:

: 15626-54-7
2-diazo-3-phenyl-propionic acid ethyl ester

: 1443117-65-4
(2S,3S,4S,5R)-2-benzyl-2,4-bis(hydroxymethyl)-3-methyl-5-phenyltetrahydrofuran

Guidance literature:: Multi-step reaction with 3 steps

1: rhodium(II) pivalate / dichloromethane / 1.17 h / -78 °C / Molecular sieve

2: sodium tetrahydroborate / tetrahydrofuran; water / 20 h / 20 °C

3: lithium aluminium tetrahydride / diethyl ether / 2 h / 20 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; rhodium(II) pivalate; In tetrahydrofuran; diethyl ether; dichloromethane; water;
DOI:10.1021/jo400858u