tri-tert-butyl 2,2',2''-(10-(2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

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Chemical Name:tri-tert-butyl 2,2',2''-(10-(2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate
CAS No.:1332625-40-7
Molecular Formula:C₄₈H₈₃N₅O₁₂
Molecular Weight:922.213
Hs Code.:

Synonyms:tri-tert-butyl 2,2',2''-(10-(2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

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Chemical Property of tri-tert-butyl 2,2',2''-(10-(2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

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Technology Process of tri-tert-butyl 2,2',2''-(10-(2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

There total 2 articles about tri-tert-butyl 2,2',2''-(10-(2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: C₃₆H₆₃N₅O₈

: 1332625-40-7
tri-tert-butyl 2,2',2''-(10-(2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

Guidance literature:: C₃₆H₆₃N₅O₈; With potassium carbonate; In acetonitrile; at 20 ℃; for 0.333333h;

bromoacetic acid tert-butyl ester; In acetonitrile; at 70 ℃;
DOI:10.1039/c1ob05463e

Reference yield:

: 1332625-39-4
tri-tert-butyl 2,2',2''-(10-(2-(2-(2-(benzyloxycarbonylamino)ethoxy)phenoxy)ethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

: 1332625-40-7
tri-tert-butyl 2,2',2''-(10-(2-(2-(2-(bis(2-tert-butoxy-2-oxoethyl)amino)ethoxy)phenoxy)ethyl)-1,4,7,10-tetraazacyclododecane-1,4,7-triyl)triacetate

Guidance literature:: Multi-step reaction with 2 steps

1.1: palladium on activated charcoal; hydrogen / ethanol / 12 h / 2250.23 Torr

2.1: potassium carbonate / acetonitrile / 0.33 h / 20 °C

2.2: 70 °C

With palladium on activated charcoal; hydrogen; potassium carbonate; In ethanol; acetonitrile;
DOI:10.1039/c1ob05463e