3-(2-methylthio-5-methyl-3-thienyl)-4,5-dihydroisoxazole-4,5-dicarboxylic acid N-phenylimide

Base Information

Chemical Name:3-(2-methylthio-5-methyl-3-thienyl)-4,5-dihydroisoxazole-4,5-dicarboxylic acid N-phenylimide
CAS No.:118554-98-6
Molecular Formula:C₁₇H₁₄N₂O₃S₂
Molecular Weight:358.442
Hs Code.:

Synonyms:3-(2-methylthio-5-methyl-3-thienyl)-4,5-dihydroisoxazole-4,5-dicarboxylic acid N-phenylimide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(2-methylthio-5-methyl-3-thienyl)-4,5-dihydroisoxazole-4,5-dicarboxylic acid N-phenylimide

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Technology Process of 3-(2-methylthio-5-methyl-3-thienyl)-4,5-dihydroisoxazole-4,5-dicarboxylic acid N-phenylimide

There total 2 articles about 3-(2-methylthio-5-methyl-3-thienyl)-4,5-dihydroisoxazole-4,5-dicarboxylic acid N-phenylimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 941-69-5
N-phenyl-maleimide

: 118554-96-4
2-methylthio-5-methylthiophene-3-aldehyde oxime

: 118554-98-6
3-(2-methylthio-5-methyl-3-thienyl)-4,5-dihydroisoxazole-4,5-dicarboxylic acid N-phenylimide

Guidance literature:: With sodium hypochlorite; triethylamine; In dichloromethane; water; 1) -5 deg C, 1 h 2) without cooling, 1 h;
DOI:10.1007/BF00475335

Reference yield:

: 100216-96-4
2-methylthio-5-methylthiophene-3-aldehyde

: 118554-98-6
3-(2-methylthio-5-methyl-3-thienyl)-4,5-dihydroisoxazole-4,5-dicarboxylic acid N-phenylimide

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / NH₂OH / ethanol; H₂O / 1.5 h / Heating

2: 90 percent / triethylamine, NaOCl / CH₂Cl₂; H₂O / 1) -5 deg C, 1 h 2) without cooling, 1 h

With sodium hypochlorite; hydroxylamine; triethylamine; In ethanol; dichloromethane; water;
DOI:10.1007/BF00475335