C₁₅H₁₈O₃

Base Information

Chemical Name:C₁₅H₁₈O₃
CAS No.:1195988-17-0
Molecular Formula:C₁₅H₁₈O₃
Molecular Weight:246.306
Hs Code.:

C<sub>15</sub>H<sub>18</sub>O<sub>3</sub>

Synonyms:C₁₅H₁₈O₃

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Chemical Property of C₁₅H₁₈O₃

Chemical Property:

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Technology Process of C₁₅H₁₈O₃

There total 1 articles about C₁₅H₁₈O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1195988-27-2
C₂₂H₂₆O₆S

: 1195988-17-0
C₁₅H₁₈O₃

Guidance literature:: With potassium carbonate; In methanol; at 20 ℃; for 4h;
DOI:10.1021/ol902217q

Reference yield:

: 1195988-17-0
C₁₅H₁₈O₃

: 2622-05-1
allylmagnesium bromide

: 1195988-28-3
C₁₈H₂₄O₃

Guidance literature:: allylmagnesium bromide; With copper(l) iodide; In tetrahydrofuran; at -40 ℃; for 0.5h;

C₁₅H₁₈O₃; In tetrahydrofuran; at -40 ℃; for 1.5h;
DOI:10.1021/ol902217q

Reference yield:

: 1195988-17-0
C₁₅H₁₈O₃

: C₃₂H₄₈O₆Si

: 1263144-07-5
C₃₂H₄₈O₆Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: copper(l) iodide / tetrahydrofuran / 1.5 h / -40 °C

2.1: dmap; triethylamine / 2.5 h / 20 °C

3.1: osmium(VIII) oxide; AD-mix-β; 1,4-bis(9-O-dihydroquinidine)phthalazine / water; tert-butyl alcohol / 70 h / 0 - 20 °C

4.1: silica-supported sodium periodate / dichloromethane / 0.67 h / 0 - 20 °C

5.1: tetrahydrofuran / 13.83 h / -40 °C

6.1: diisobutylaluminium hydride / hexane; dichloromethane / 0.33 h / -78 °C

6.2: -78 - 20 °C

7.1: titanium(IV) isopropylate; tert.-butylhydroperoxide; diethyl (2S,3S)-tartrate / dichloromethane / 44 h / -40 - -15 °C / Molecular sieve

7.2: 3 h / -15 - 20 °C

8.1: silver nitrate; triethylamine / tetrahydrofuran / 0.75 h / 0 °C

8.2: 15 h / 0 - 20 °C

9.1: camphor-10-sulfonic acid / methanol; dichloromethane / 2.5 h / 0 - 20 °C

10.1: dimethyl sulfoxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / 3 h / 20 °C

11.1: potassium hexamethylsilazane / 1,2-dimethoxyethane / 0.5 h / -75 - -65 °C

11.2: 3 h / -75 - 0 °C

With titanium(IV) isopropylate; tert.-butylhydroperoxide; dmap; copper(l) iodide; osmium(VIII) oxide; diethyl (2S,3S)-tartrate; silica-supported sodium periodate; AD-mix-β; camphor-10-sulfonic acid; potassium hexamethylsilazane; diisobutylaluminium hydride; silver nitrate; dimethyl sulfoxide; 1,4-bis(9-O-dihydroquinidine)phthalazine; triethylamine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; hexane; dichloromethane; water; tert-butyl alcohol; 5.1: Wittig reaction / 7.1: Sharpless epoxidation / 11.1: Julia-Kocienski reaction / 11.2: Julia-Kocienski reaction;
DOI:10.1016/j.tet.2010.11.017