C₃₂H₃₆O₉N₆C₂₀H₂₅O₅F₃

Base Information

Chemical Name:C₃₂H₃₆O₉N₆C₂₀H₂₅O₅F₃
CAS No.:1053716-25-8
Molecular Formula:C₅₂H₆₁F₃N₆O₁₄
Molecular Weight:1051.08
Hs Code.:

C<sub>32</sub>H<sub>36</sub>O<sub>9</sub>N<sub>6</sub>C<sub>20</sub>H<sub>25</sub>O<sub>5</sub>F<sub>3</sub>

Synonyms:C₃₂H₃₆O₉N₆C₂₀H₂₅O₅F₃

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Chemical Property of C₃₂H₃₆O₉N₆C₂₀H₂₅O₅F₃

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Technology Process of C₃₂H₃₆O₉N₆C₂₀H₂₅O₅F₃

There total 6 articles about C₃₂H₃₆O₉N₆C₂₀H₂₅O₅F₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 277317-38-1
C₃₂H₃₅O₉N₅IC₂₀H₂₅O₅NF₃

: 1053716-25-8
C₃₂H₃₆O₉N₆C₂₀H₂₅O₅F₃

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 2h;
DOI:10.1021/ol005696f

Reference yield:

: 3587-60-8
Benzyloxymethyl chloride

: 1053716-25-8
C₃₂H₃₆O₉N₆C₂₀H₂₅O₅F₃

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / BEMP / tetrahydrofuran / 45 h / 0 °C

2: 85 percent / HCl; Na(CN)BH₃; molecular sieves 3 Angstroem / tetrahydrofuran; diethyl ether

3: 78 percent / N-iodosuccinimide; TfOH; molecular sieves 3 Angstroem / 1,2-dichloro-ethane / 0.67 h / 20 °C

4: 80 percent / H₂ / Pd/C / ethyl acetate / 2 h / 20 °C

With hydrogenchloride; N-iodo-succinimide; trifluorormethanesulfonic acid; 3 A molecular sieve; hydrogen; sodium cyanoborohydride; 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethyl acetate; 1,2-dichloro-ethane; 1: Addition / 2: Hydrolysis / 3: Glycosylation / 4: Dehalogenation;
DOI:10.1021/ol005696f

Reference yield:

: 154706-36-2
2,2-Dimethyl-propionic acid (2S,4aR,5aR,6R,7R,8aR,9R,9aR)-9-azido-2-phenyl-7-phenylsulfanyl-octahydro-furo[2',3':5,6]pyrano[3,2-d][1,3]dioxin-6-yl ester

: 1053716-25-8
C₃₂H₃₆O₉N₆C₂₀H₂₅O₅F₃

Guidance literature:: Multi-step reaction with 5 steps

1: 65 percent / N-iodosuccinimide; TfOH / 1,2-dichloro-ethane / 2.5 h / 20 °C

2: 95 percent / BEMP / tetrahydrofuran / 45 h / 0 °C

3: 85 percent / HCl; Na(CN)BH₃; molecular sieves 3 Angstroem / tetrahydrofuran; diethyl ether

4: 78 percent / N-iodosuccinimide; TfOH; molecular sieves 3 Angstroem / 1,2-dichloro-ethane / 0.67 h / 20 °C

5: 80 percent / H₂ / Pd/C / ethyl acetate / 2 h / 20 °C

With hydrogenchloride; N-iodo-succinimide; trifluorormethanesulfonic acid; 3 A molecular sieve; hydrogen; sodium cyanoborohydride; 2-tert-butylimino-2-diethylamino-1,3-dimethyl-perhydro-1,3,2-diazaphosphorine; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; ethyl acetate; 1,2-dichloro-ethane; 1: Substitution / 2: Addition / 3: Hydrolysis / 4: Glycosylation / 5: Dehalogenation;
DOI:10.1021/ol005696f