5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylidenamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide

Base Information

• Chemical Name: 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylidenamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide
• CAS No.: 329325-93-1
• Molecular Formula: C₆₈H₆₈N₄O₈S₄
• Molecular Weight: 1197.57

Synonyms:5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylidenamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide

Chemical Property of 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylidenamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide

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Technology Process of 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylidenamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide

There total 4 articles about 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylidenamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetramethoxy-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide (329325-92-0) → 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylidenamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide (329325-93-1)

Guidance literature:

With N-Bromosuccinimide; dibenzoyl peroxide; In benzene; for 1h; Heating;

DOI:10.1021/ja005573q

Reference yield:

benzylamine (100-46-9) → 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylidenamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide (329325-93-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

1.2: 64 percent / tetrahydrofuran; hexane / 2 h / 20 °C

2.1: 87 percent / H₂O₂ / CHCl₃; trifluoroacetic acid / 17 h / Heating

3.1: 90 percent / N-bromosuccinimide; dibenzoyl peroxide / benzene / 1 h / Heating

With N-Bromosuccinimide; n-butyllithium; dihydrogen peroxide; dibenzoyl peroxide; In tetrahydrofuran; hexane; chloroform; trifluoroacetic acid; benzene;

DOI:10.1021/ja005573q

Reference yield:

5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetramethoxy-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,8,14,20-tetraoxide (204190-45-4,518034-43-0,518034-44-1,518034-45-2,518034-46-3) → 5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylidenamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1(25),3,5,7(28),9,11,13(27),15,17,19(26),21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide (329325-93-1)

Guidance literature:

Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C

1.2: 64 percent / tetrahydrofuran; hexane / 2 h / 20 °C

2.1: 87 percent / H₂O₂ / CHCl₃; trifluoroacetic acid / 17 h / Heating

3.1: 90 percent / N-bromosuccinimide; dibenzoyl peroxide / benzene / 1 h / Heating

With N-Bromosuccinimide; n-butyllithium; dihydrogen peroxide; dibenzoyl peroxide; In tetrahydrofuran; hexane; chloroform; trifluoroacetic acid; benzene;

DOI:10.1021/ja005573q

upstream raw materials:

5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetramethoxy-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,2,8,8,14,14,20,20-octaoxide

benzylamine

5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetramethoxy-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide

5,11,17,23-tetrakis(1,1-dimethylethyl)-25,26,27,28-tetrakis(N-benzylamino)-2,8,14,20-tetrathiapentacyclo[19.3.1.1(3,7).1(9,13).1(15,19)]octacosa-1⁽²⁵⁾,3,5,7⁽²⁸⁾,9,11,13⁽²⁷⁾,15,17,19⁽²⁶⁾,21,23-dodecaene-2,8,14,20-tetraoxide

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