4-[2-(N-ethcmcarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-1,1-dioxide-3-one

Base Information

Chemical Name:4-[2-(N-ethcmcarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-1,1-dioxide-3-one
CAS No.:1251834-73-7
Molecular Formula:C₁₅H₁₇F₃N₂O₇S₂
Molecular Weight:458.436
Hs Code.:

Synonyms:4-[2-(N-ethcmcarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-1,1-dioxide-3-one

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Chemical Property of 4-[2-(N-ethcmcarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-1,1-dioxide-3-one

Chemical Property:

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Technology Process of 4-[2-(N-ethcmcarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-1,1-dioxide-3-one

There total 4 articles about 4-[2-(N-ethcmcarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-1,1-dioxide-3-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1251834-72-6
4-[2-(N-ethoxycarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-3-one

: 1251834-73-7
4-[2-(N-ethcmcarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-1,1-dioxide-3-one

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 2h;

Reference yield:

: 1251834-71-5
4-(2-trifluoromethanesulfonylaminobenzyl)-1,4-thiazinan-3-one

: 1251834-73-7
4-[2-(N-ethcmcarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-1,1-dioxide-3-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / acetonitrile / 2 h / Reflux

2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C

With sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; acetonitrile;

Reference yield:

: 5344-90-1
2-Aminobenzyl alcohol

: 1251834-73-7
4-[2-(N-ethcmcarbonyl-N-trifluoromethanesulfonyl)aminobenzyl]-1,4-thiazinan-1,1-dioxide-3-one

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / chloroform / 4 h / 0 - 20 °C

2: toluene-4-sulfonic acid / m-xylene / 3 h / Reflux

3: sodium hydrogencarbonate / acetonitrile / 2 h / Reflux

4: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 2 h / 20 °C

With sodium hydrogencarbonate; toluene-4-sulfonic acid; triethylamine; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; chloroform; m-xylene; acetonitrile;