2-(4-methoxyphenyl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)(2,1-d)-2-thiazoline hydrobromide

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Chemical Name:2-(4-methoxyphenyl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)(2,1-d)-2-thiazoline hydrobromide
CAS No.:109947-50-4
Molecular Formula:BrH*C₂₀H₂₄N₂O₈S
Molecular Weight:533.397
Hs Code.:

Synonyms:2-(4-methoxyphenyl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)(2,1-d)-2-thiazoline hydrobromide

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Chemical Property of 2-(4-methoxyphenyl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)(2,1-d)-2-thiazoline hydrobromide

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Technology Process of 2-(4-methoxyphenyl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)(2,1-d)-2-thiazoline hydrobromide

There total 3 articles about 2-(4-methoxyphenyl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)(2,1-d)-2-thiazoline hydrobromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 110012-64-1
1,3,4,6-tetra-O-acetyl-2-deoxy-2-<3-(4-methoxyphenyl)thioureido>-α-D-glucopyranose

: 109947-50-4
2-(4-methoxyphenyl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)(2,1-d)-2-thiazoline hydrobromide

Guidance literature:: With hydrogen bromide; In acetic acid; for 2h; Ambient temperature;
DOI:10.1016/S0008-6215(00)90021-1

Reference yield:

: 109947-42-4
1,3,4,6-Tetra-O-acetyl-2-deoxy-2-isothiocyanato-α-D-glucopyranose

: 109947-50-4
2-(4-methoxyphenyl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)(2,1-d)-2-thiazoline hydrobromide

Guidance literature:: Multi-step reaction with 2 steps

1: 68 percent / diethyl ether / 24 h / Ambient temperature

2: 83 percent / HBr / acetic acid / 2 h / Ambient temperature

With hydrogen bromide; In diethyl ether; acetic acid;
DOI:10.1016/S0008-6215(00)90021-1

Reference yield:

: 10034-19-2,1191127-63-5
1,3,4,6-tetra-O-acetyl-2-amino-2-deoxy-α-D-glucopyranose hydrochloride

: 109947-50-4
2-(4-methoxyphenyl)amino-(3,4,6-tri-O-acetyl-1,2-dideoxy-α-D-glucopyrano)(2,1-d)-2-thiazoline hydrobromide

Guidance literature:: Multi-step reaction with 3 steps

1: 54 percent / calcium carbonate / CHCl₃; H₂O / 48 h

2: 68 percent / diethyl ether / 24 h / Ambient temperature

3: 83 percent / HBr / acetic acid / 2 h / Ambient temperature

With hydrogen bromide; calcium carbonate; In diethyl ether; chloroform; water; acetic acid;
DOI:10.1016/S0008-6215(00)90021-1