Technology Process of C24H42O3S2Si
There total 5 articles about C24H42O3S2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C16H34O2S2Si;
With
sodium hydride;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 0.5h;
Inert atmosphere;
p-methoxybenzyl chloride;
In
tetrahydrofuran; N,N-dimethyl-formamide; mineral oil;
at 0 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/ol2007296
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sulfur trioxide pyridine complex; triethylamine / dichloromethane; dimethyl sulfoxide / 3 h / 0 °C / Inert atmosphere
2.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -20 °C / Inert atmosphere
2.2: -78 °C / Inert atmosphere
3.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere
3.2: 4 h / 0 °C / Inert atmosphere
With
n-butyllithium; sulfur trioxide pyridine complex; sodium hydride; triethylamine;
In
tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol2007296
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 1 h / -20 °C / Inert atmosphere
1.2: -78 °C / Inert atmosphere
2.1: sodium hydride / tetrahydrofuran; N,N-dimethyl-formamide; mineral oil / 0.5 h / 0 °C / Inert atmosphere
2.2: 4 h / 0 °C / Inert atmosphere
With
n-butyllithium; sodium hydride;
In
tetrahydrofuran; hexane; N,N-dimethyl-formamide; mineral oil;
DOI:10.1021/ol2007296
