Technology Process of C54H55N13O10S6
There total 4 articles about C54H55N13O10S6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine; dmap;
In
dichloromethane;
for 3h;
DOI:10.1021/jm101602q
- Guidance literature:
-
Multi-step reaction with 6 steps
1: formic acid
2: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
3: triethylamine / acetone / Sonication
4: sodium azide / acetone / 1.33 h / 60 °C
5: 14 h / 80 °C
6: pyridine; dmap / dichloromethane / 3 h
With
pyridine; dmap; formic acid; sodium azide; water; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; acetone;
5: Curtius rearrangement;
DOI:10.1021/jm101602q
- Guidance literature:
-
Multi-step reaction with 5 steps
1: water; sodium hydroxide / tetrahydrofuran / 1.5 h / 60 °C
2: triethylamine / acetone / Sonication
3: sodium azide / acetone / 1.33 h / 60 °C
4: 14 h / 80 °C
5: pyridine; dmap / dichloromethane / 3 h
With
pyridine; dmap; sodium azide; water; triethylamine; sodium hydroxide;
In
tetrahydrofuran; dichloromethane; acetone;
4: Curtius rearrangement;
DOI:10.1021/jm101602q