(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester

Base Information

Chemical Name:(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester
CAS No.:1051966-61-0
Molecular Formula:C₃₆H₆₀O₅S₂
Molecular Weight:637.001
Hs Code.:

Synonyms:(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester

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Chemical Property of (+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester

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Technology Process of (+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester

There total 1 articles about (+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 112-92-5
1-octadecanol

: 1051966-45-0
(+/-)-6-(2-hydroxy-3-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]-dithian-2-yl}-propyl)-2,2-dimethyl-[1,3]-dioxin-4-one

: 1051966-61-0
(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester

Guidance literature:: In toluene; at 110 ℃; for 6h;
DOI:10.1021/jm8007322

Reference yield: 84.0%

: 1051966-61-0
(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester

: (+/-)-(3R*,5R*)-3,5-dihydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-hexanoic acid octadecyl ester

Guidance literature:: With tetramethylammonium triacetoxyborohydride; In dichloromethane; acetic acid; acetonitrile; at 0 ℃; for 3h;

Reference yield: 57.0%

: 1051966-61-0
(+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester

: (+/-)-(3R*,5S*)-3,5-dihydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-hexanoic acid octadecyl ester

Guidance literature:: (+/-)-5-hydroxy-6-{2-[2-(4-hydroxyphenyl)-ethyl]-[1,3]dithian-2-yl}-3-oxohexanoic acid octadecyl ester; With triethyl borane; In tetrahydrofuran; methanol; hexane; at 20 ℃; for 1h;

With sodium tetrahydroborate; In tetrahydrofuran; methanol; hexane; at -78 ℃; for 2h;
DOI:10.1021/jm8007322