(N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

Base Information

Chemical Name:(N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester
CAS No.:85479-38-5
Molecular Formula:C₃₄H₄₂N₆O₈
Molecular Weight:662.743
Hs Code.:

Synonyms:(N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

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Chemical Property of (N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

Chemical Property:

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Technology Process of (N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

There total 1 articles about (N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2130-96-3,54784-43-9
O-benzyl-N-tert-butoxycarbonyl-L-tyrosine

: 7672-27-7
N'-nitro-L-arginine benzyl ester

: 85479-38-5
(N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; Yield given. Multistep reaction; 1.) DMF, 20 min, 2.) -20 deg C, 3 h;
DOI:10.1021/ja00350a054

Reference yield: 94.0%

: 85479-38-5
(N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

: 85479-39-6
C₂₉H₃₄N₆O₆*ClH

Guidance literature:: With hydrogenchloride; In 1,4-dioxane; for 0.5h; Ambient temperature;
DOI:10.1021/ja00350a054

Reference yield:

: 85479-38-5
(N-tert-butyloxycarbonyl-O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

: 85479-40-9
(O-benzyl-L-tyrosyl)-N'-nitro-L-arginine benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / HCl / dioxane / 0.5 h / Ambient temperature

2: 1.) isobutyl chloroformate, N-methylmorpholine / 1.) DMF, 25 min, 2.) -25 deg C, 3 h

With 4-methyl-morpholine; hydrogenchloride; isobutyl chloroformate; In 1,4-dioxane;
DOI:10.1021/ja00350a054