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5-(4-[tert-butyl(dimethyl)silyloxy]phenyl)-3-[4'-(trifluoromethyl)phenyl]-2-pyrazinamine

Base Information Edit
  • Chemical Name:5-(4-[tert-butyl(dimethyl)silyloxy]phenyl)-3-[4'-(trifluoromethyl)phenyl]-2-pyrazinamine
  • CAS No.:625848-38-6
  • Molecular Formula:C23H26F3N3OSi
  • Molecular Weight:445.56
  • Hs Code.:
  • Mol file:625848-38-6.mol
5-(4-[tert-butyl(dimethyl)silyloxy]phenyl)-3-[4'-(trifluoromethyl)phenyl]-2-pyrazinamine

Synonyms:5-(4-[tert-butyl(dimethyl)silyloxy]phenyl)-3-[4'-(trifluoromethyl)phenyl]-2-pyrazinamine

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Chemical Property of 5-(4-[tert-butyl(dimethyl)silyloxy]phenyl)-3-[4'-(trifluoromethyl)phenyl]-2-pyrazinamine Edit
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Technology Process of 5-(4-[tert-butyl(dimethyl)silyloxy]phenyl)-3-[4'-(trifluoromethyl)phenyl]-2-pyrazinamine

There total 3 articles about 5-(4-[tert-butyl(dimethyl)silyloxy]phenyl)-3-[4'-(trifluoromethyl)phenyl]-2-pyrazinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With bis(benzonitrile)palladium(II) dichloride; sodium carbonate; 1,4-di(diphenylphosphino)-butane; In ethanol; water; toluene; for 0.116667h; Heating;
DOI:10.1016/j.tet.2003.08.040
Guidance literature:
With bis(benzonitrile)palladium(II) dichloride; sodium carbonate; 1,4-di(diphenylphosphino)-butane; In ethanol; water; toluene; at 20 ℃; for 15.5h; Reflux; Inert atmosphere;
DOI:10.1016/j.bmc.2009.05.025
Guidance literature:
Multi-step reaction with 2 steps
1: 41 percent / 1,4-bis(diphenylphosphino)butane; (PhCN)2PdCl2; Na2CO3 / toluene; ethanol; H2O / 7 h / Heating
2: 92 percent / 1,4-bis(diphenylphospino)butane; (PhCN)2PdCl2; Na2CO3 / toluene; ethanol; H2O / 0.12 h / Heating
With bis(benzonitrile)palladium(II) dichloride; sodium carbonate; 1,4-di(diphenylphosphino)-butane; In ethanol; water; toluene; 1: Suzuki coupling / 2: Suzuki coupling;
DOI:10.1016/j.tet.2003.08.040
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