diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester

Base Information

Chemical Name:diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester
CAS No.:1313715-55-7
Molecular Formula:C₄₅H₅₁N₂O₇P
Molecular Weight:762.883
Hs Code.:

diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester

Synonyms:diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester

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Chemical Property of diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester

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Technology Process of diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester

There total 4 articles about diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 1313715-54-6
2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-ol

: 124482-92-4,89992-70-1
2-cyanoethyl-N,N-(diisopropylamino)chlorophosphine

: 1313715-55-7
diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1002/chem.201100067

Reference yield:

: 872051-17-7
1-β-(4-bromophenyl)-1,2-dideoxy-3,5-di-O-(4-toluoyl)-D-ribofuranose

: 1313715-55-7
diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / N,N-dimethyl-formamide / 18 h / 100 °C / Inert atmosphere

2: sodium methylate / methanol / 20 °C

3: pyridine / 20 °C / Cooling with ice

4: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; sodium methylate; N-ethyl-N,N-diisopropylamine; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide; 1: Stille coupling;
DOI:10.1002/chem.201100067

Reference yield:

: 1313715-52-4
1,2-dideoxy-1β-[4-(2-furyl)phenyl]-3,5-di-O-(4-toluoyl)-D-ribofuranose

: 1313715-55-7
diisopropylamidophosphorous acid 2-[bis(4-methoxyphenyl)(phenyl)methoxymethyl]-5-[4-(furan-2-yl)phenyl]tetrahydrofuran-3-yl ester 2-cyanoethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: sodium methylate / methanol / 20 °C

2: pyridine / 20 °C / Cooling with ice

3: N-ethyl-N,N-diisopropylamine / dichloromethane / 2 h / 20 °C

With sodium methylate; N-ethyl-N,N-diisopropylamine; In pyridine; methanol; dichloromethane;
DOI:10.1002/chem.201100067