(11β,17α)-17-{[4-(3-chloro-4-hydroxyphenoxy)benzoyl]oxy}-9-fluoro-11-hydroxy-3-oxoandrosta-1,4-diene-17-carbothioic S-acid

Base Information

Chemical Name:(11β,17α)-17-{[4-(3-chloro-4-hydroxyphenoxy)benzoyl]oxy}-9-fluoro-11-hydroxy-3-oxoandrosta-1,4-diene-17-carbothioic S-acid
CAS No.:1257087-27-6
Molecular Formula:C₃₃H₃₂ClFO₇S
Molecular Weight:627.13
Hs Code.:

Synonyms:(11β,17α)-17-{[4-(3-chloro-4-hydroxyphenoxy)benzoyl]oxy}-9-fluoro-11-hydroxy-3-oxoandrosta-1,4-diene-17-carbothioic S-acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (11β,17α)-17-{[4-(3-chloro-4-hydroxyphenoxy)benzoyl]oxy}-9-fluoro-11-hydroxy-3-oxoandrosta-1,4-diene-17-carbothioic S-acid

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Technology Process of (11β,17α)-17-{[4-(3-chloro-4-hydroxyphenoxy)benzoyl]oxy}-9-fluoro-11-hydroxy-3-oxoandrosta-1,4-diene-17-carbothioic S-acid

There total 1 articles about (11β,17α)-17-{[4-(3-chloro-4-hydroxyphenoxy)benzoyl]oxy}-9-fluoro-11-hydroxy-3-oxoandrosta-1,4-diene-17-carbothioic S-acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

: 1257087-05-0
4-(4-acetoxy-3-chlorophenoxy)benzoic acid

: 80473-91-2
9α-fluoro-11β,17α-dihydroxy-3-oxoandrosta-1,4-diene-17β-carbothioic acid

: 1257087-27-6
(11β,17α)-17-{[4-(3-chloro-4-hydroxyphenoxy)benzoyl]oxy}-9-fluoro-11-hydroxy-3-oxoandrosta-1,4-diene-17-carbothioic S-acid

Guidance literature:: 4-(4-acetoxy-3-chlorophenoxy)benzoic acid; With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 0 - 20 ℃;

9α-fluoro-11β,17α-dihydroxy-3-oxoandrosta-1,4-diene-17β-carbothioic acid; In N,N-dimethyl-formamide; at 20 ℃; for 18h;

With hydrogenchloride; sodium hydrogencarbonate; In methanol; water; at 20 ℃; for 7h; pH=7;