5'-{3-[2-(1,3-dioxan-2-yl)phenyl]propylthio}-4'-methyl-4,5-ethylenedithiotetrathiafulvalene

Base Information

Chemical Name:5'-{3-[2-(1,3-dioxan-2-yl)phenyl]propylthio}-4'-methyl-4,5-ethylenedithiotetrathiafulvalene
CAS No.:564469-04-1
Molecular Formula:C₂₂H₂₄O₂S₇
Molecular Weight:544.893
Hs Code.:

Synonyms:5'-{3-[2-(1,3-dioxan-2-yl)phenyl]propylthio}-4'-methyl-4,5-ethylenedithiotetrathiafulvalene

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Chemical Property of 5'-{3-[2-(1,3-dioxan-2-yl)phenyl]propylthio}-4'-methyl-4,5-ethylenedithiotetrathiafulvalene

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Technology Process of 5'-{3-[2-(1,3-dioxan-2-yl)phenyl]propylthio}-4'-methyl-4,5-ethylenedithiotetrathiafulvalene

There total 1 articles about 5'-{3-[2-(1,3-dioxan-2-yl)phenyl]propylthio}-4'-methyl-4,5-ethylenedithiotetrathiafulvalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 171086-95-6
2-<2-(4-Iodopropanyl)phenyl>-1,3-dioxane

: 4-(2-cyanoethylthio)-5-methyl-4′,5′-ethylenedithiotetrathiafulvalene

: 564469-04-1
5'-{3-[2-(1,3-dioxan-2-yl)phenyl]propylthio}-4'-methyl-4,5-ethylenedithiotetrathiafulvalene

Guidance literature:: 4-(2-cyanoethylthio)-5-methyl-4′,5′-ethylenedithiotetrathiafulvalene; With sodium methylate; In methanol; at 20 ℃;

2-<2-(4-Iodopropanyl)phenyl>-1,3-dioxane; In methanol; at 20 ℃; for 2h;
DOI:10.1021/jp037145n

Reference yield: 89.0%

: 564469-04-1
5'-{3-[2-(1,3-dioxan-2-yl)phenyl]propylthio}-4'-methyl-4,5-ethylenedithiotetrathiafulvalene

: 564469-07-4
5'-[3-(2-formylphenyl)propylthio]-4'-methyl-4,5-ethylenedithiotetrathiafulvalene

Guidance literature:: With pyridinium p-toluenesulfonate; In acetone; Heating;
DOI:10.1021/jp037145n

Reference yield:

: 564469-04-1
5'-{3-[2-(1,3-dioxan-2-yl)phenyl]propylthio}-4'-methyl-4,5-ethylenedithiotetrathiafulvalene

: 2-{4-[3-(2-diazomethyl-phenyl)-propylsulfanyl]-5-methyl-[1,3]dithiol-2-ylidene}-5,6-dihydro-[1,3]dithiolo[4,5-b][1,4]dithiine

Guidance literature:: Multi-step reaction with 3 steps

1: 89 percent / aq. pyridinium p-toluenesulfonic acid / acetone / Heating

2: 80 percent / tetrahydrofuran / 2 h / Heating

3: NaOMe / methanol / 0.17 h / Heating

With sodium methylate; pyridinium p-toluenesulfonate; In tetrahydrofuran; methanol; acetone;
DOI:10.1021/jp037145n