C₂₁H₂₄O₆S

Base Information

• Chemical Name: C₂₁H₂₄O₆S
• CAS No.: 1256640-06-8
• Molecular Formula: C₂₁H₂₄O₆S
• Molecular Weight: 404.484
• Mol file: 1256640-06-8.mol

Synonyms:C₂₁H₂₄O₆S

Chemical Property of C₂₁H₂₄O₆S

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₁H₂₄O₆S

There total 13 articles about C₂₁H₂₄O₆S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

C28H30O6S (1256640-05-7) → C21H24O6S (1256640-06-8)

Guidance literature:

With palladium 10% on activated carbon; hydrogen; In tetrahydrofuran; at 20 ℃; for 2.5h;

DOI:10.1002/chem.201400131

Reference yield:

C29H34O6S (1256640-02-4) → C21H24O6S (1256640-06-8)

Guidance literature:

Multi-step reaction with 4 steps

1.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide / tetrahydrofuran; water; tert-butyl alcohol / 12 h / 20 °C

2.1: sodium periodate / tetrahydrofuran; water / 2 h / 20 °C

3.1: lithium perchlorate / dichloromethane / 0.75 h / 20 °C / Molecular sieve; Inert atmosphere

3.2: 3.5 h / 20 °C / Inert atmosphere

4.1: 10% palladium on activated carbon; hydrogen / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

With sodium periodate; osmium(VIII) oxide; 10% palladium on activated carbon; hydrogen; lithium perchlorate; 4-methylmorpholine N-oxide; In tetrahydrofuran; dichloromethane; water; tert-butyl alcohol; 3.1: Friedel Crafts acylation / 3.2: Friedel Crafts acylation;

DOI:10.1021/ol102390t

Reference yield:

C28H32O7S (1256640-04-6) → C21H24O6S (1256640-06-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium perchlorate / dichloromethane / 0.75 h / 20 °C / Molecular sieve; Inert atmosphere

1.2: 3.5 h / 20 °C / Inert atmosphere

2.1: 10% palladium on activated carbon; hydrogen / tetrahydrofuran / 2.5 h / 20 °C / Inert atmosphere

With 10% palladium on activated carbon; hydrogen; lithium perchlorate; In tetrahydrofuran; dichloromethane; 1.1: Friedel Crafts acylation / 1.2: Friedel Crafts acylation;

DOI:10.1021/ol102390t

upstream raw materials:

C₁₉H₂₂O₄

C₂₂H₂₈O₄

C₂₉H₃₄O₆S

C₂₉H₃₆O₈S