Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

Base Information

Chemical Name:Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate
CAS No.:123910-96-3
Molecular Formula:C₃₁H₃₉N₅O₇
Molecular Weight:593.68
Hs Code.:

Synonyms:Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

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Chemical Property of Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

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Technology Process of Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

There total 2 articles about Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1118-89-4
diethyl-L-glutamate hydrochloride

: 123910-94-1
4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoic acid

: 123910-96-3
Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

Guidance literature:: With 4-methyl-morpholine; 1-methyl-pyrrolidin-2-one; Phenyl N-phenylphosphoramidochloridate; for 24h; Ambient temperature;
DOI:10.1021/jo00297a044

Reference yield:

: 126295-77-0
C₂₇H₃₂N₄O₅

: 123910-96-3
Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

Guidance literature:: Multi-step reaction with 2 steps

1: 1 N NaOH / H₂O

2: 35 percent / phenyl N-phenylphosphoramidochloridate, N-methylmorpholine, N-methylpyrrolidinone / 24 h / Ambient temperature

With 4-methyl-morpholine; 1-methyl-pyrrolidin-2-one; sodium hydroxide; Phenyl N-phenylphosphoramidochloridate; In water;
DOI:10.1021/jo00297a044

Reference yield: 100.0%

: 123910-96-3
Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4-dihydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

: 123910-97-4
Diethyl N-<4-<3-<2-(Pivaloylamino)-3,4,5,6,7,8-hexahydro-4-oxo-5-deazapteridin-6-yl>propyl>benzoyl>-L-glutamate

Guidance literature:: With hydrogen; palladium on activated charcoal; In trifluoroacetic acid; for 24h; under 2585.7 Torr;
DOI:10.1021/jo00297a044