phenyl exo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside

Base Information

Chemical Name:phenyl exo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside
CAS No.:158716-04-2
Molecular Formula:C₂₆H₂₄O₅S
Molecular Weight:448.54
Hs Code.:

Synonyms:phenyl exo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside

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Chemical Property of phenyl exo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside

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Technology Process of phenyl exo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside

There total 1 articles about phenyl exo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1125-88-8
benzaldehyde dimethyl acetal

: 2936-70-1,5624-48-6,13992-15-9,16758-34-2,28244-97-5,77481-63-1,105088-17-3,149495-84-1,77481-62-0
(2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-phenylsulfanyl-tetrahydro-pyran-3,4,5-triol

: phenyl endo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside

: 158716-04-2
phenyl exo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In N,N-dimethyl-formamide; at 75 ℃; for 4h; Yield given;
DOI:10.1016/0008-6215(94)84264-7

Reference yield: 73.7%

: 158716-04-2
phenyl exo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside

: 158716-08-6
phenyl 4,6-O-benzylidene-2-O-benzyl-1-deoxy-1-thio-α-D-mannopyranoside

: 158716-07-5
phenyl 3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; dichloromethane; for 0.75h;
DOI:10.1016/0008-6215(94)84264-7

Reference yield:

: 158716-04-2
phenyl exo(phenyl)-2,3:4,6-di-O-benzylidene-1-thio-α-D-mannopyranoside

: 158716-09-7
phenyl 2-O-acetyl-3-O-benzyl-4,6-O-benzylidene-1-thio-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 73.7 percent / LiAlH₄, AlCl₃ / CH₂Cl₂; diethyl ether / 0.75 h

2: 91.5 percent / pyridine / Ambient temperature

With pyridine; lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; dichloromethane;
DOI:10.1016/0008-6215(94)84264-7