Technology Process of C34H34F2N2O6
There total 13 articles about C34H34F2N2O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium tetrahydroborate; diethyl methoxy borane; acetic acid;
In
tetrahydrofuran;
at -78 ℃;
for 2h;
DOI:10.1016/j.bmcl.2007.05.096
- Guidance literature:
-
Multi-step reaction with 5 steps
1: SOCl2 / 80 °C
2: Et3N / tetrahydrofuran / 12 h / 25 °C
3: toluene / 48 h / 110 °C
4: aq. HF / acetonitrile / 2 h / 0 °C
5: Et2B(OMe); NaBH4; AcOH / tetrahydrofuran / 2 h / -78 °C
With
sodium tetrahydroborate; thionyl chloride; diethyl methoxy borane; hydrogen fluoride; acetic acid; triethylamine;
In
tetrahydrofuran; toluene; acetonitrile;
3: Wittig olefination;
DOI:10.1016/j.bmcl.2007.05.096
- Guidance literature:
-
Multi-step reaction with 4 steps
1: Et3N / tetrahydrofuran / 12 h / 25 °C
2: toluene / 48 h / 110 °C
3: aq. HF / acetonitrile / 2 h / 0 °C
4: Et2B(OMe); NaBH4; AcOH / tetrahydrofuran / 2 h / -78 °C
With
sodium tetrahydroborate; diethyl methoxy borane; hydrogen fluoride; acetic acid; triethylamine;
In
tetrahydrofuran; toluene; acetonitrile;
2: Wittig olefination;
DOI:10.1016/j.bmcl.2007.05.096