menthyl-isocyanate

Base Information

Chemical Name:menthyl-isocyanate
CAS No.:39633-53-9
Molecular Formula:C₁₁H₁₉NO
Molecular Weight:181.278
Hs Code.:

Synonyms:menthyl-isocyanate

Suppliers and Price of menthyl-isocyanate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of menthyl-isocyanate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of menthyl-isocyanate

There total 11 articles about menthyl-isocyanate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 16052-40-7
(-)-(1R,3R,4S)-4-isopropyl-1-methylcyclohexane-3-carboxylic acid

: 39633-53-9
(-)-(1R,3R,4S)-menthyl isocyanate

Guidance literature:: With diphenyl phosphoryl azide; triethylamine; In DMF (N,N-dimethyl-formamide); at 0 - 20 ℃; for 5h;

Reference yield:

: 1446348-69-1
C₁₁H₁₉N

: 39633-53-9
(1R)-neomenthyl isocyanate

Guidance literature:: With pyridine N-oxide; iodine; In 1,2-dichloro-ethane; at 20 ℃; for 0.5h; Molecular sieve; Inert atmosphere;
DOI:10.1002/ejoc.201301206

Reference yield:

: 34048-58-3,57457-71-3,83213-88-1,100049-49-8
N-((1R)-neomenthyl)-formamide

: 39633-53-9
(1R)-neomenthyl isocyanate

Guidance literature:: Multi-step reaction with 2 steps

1: bis(trichloromethyl) carbonate; triethylamine / dichloromethane / 0.5 h / -20 °C

2: pyridine N-oxide; iodine / 1,2-dichloro-ethane / 0.5 h / 20 °C / Molecular sieve; Inert atmosphere

With pyridine N-oxide; bis(trichloromethyl) carbonate; iodine; triethylamine; In dichloromethane; 1,2-dichloro-ethane;
DOI:10.1002/ejoc.201301206