2-[(allyl)(5-allyl-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-N-benzyl-2-cyclopropylacetamide

Base Information

Chemical Name:2-[(allyl)(5-allyl-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-N-benzyl-2-cyclopropylacetamide
CAS No.:946088-44-4
Molecular Formula:C₂₉H₃₂N₄O
Molecular Weight:452.599
Hs Code.:

Synonyms:2-[(allyl)(5-allyl-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-N-benzyl-2-cyclopropylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-[(allyl)(5-allyl-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-N-benzyl-2-cyclopropylacetamide

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Technology Process of 2-[(allyl)(5-allyl-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-N-benzyl-2-cyclopropylacetamide

There total 2 articles about 2-[(allyl)(5-allyl-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-N-benzyl-2-cyclopropylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 255869-27-3
5-allyl-6-methyl-2-phenyl-pyrimidin-4-ol

: 88333-03-3,10340-91-7
Benzyl isocyanide

: 107-11-9,30551-89-4
1-amino-2-propene

: 1489-69-6
Cyclopropanecarboxaldehyde

: 946088-44-4
2-[(allyl)(5-allyl-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-N-benzyl-2-cyclopropylacetamide

Guidance literature:: In toluene; at 110 ℃; for 24h;
DOI:10.1021/jo070706c

Reference yield:

: 610-89-9,84984-48-5
2-acetyl-pent-4-enoic acid ethyl ester

: 946088-44-4
2-[(allyl)(5-allyl-6-methyl-2-phenyl-pyrimidin-4-yl)amino]-N-benzyl-2-cyclopropylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / NaOEt / ethanol / 80 °C

2: 70 percent / toluene / 24 h / 110 °C

With sodium ethanolate; In ethanol; toluene;
DOI:10.1021/jo070706c