ethyl-4-(2-methoxy-2-oxoethyl)-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline 5(4H)-carboxylate

Base Information

Chemical Name:ethyl-4-(2-methoxy-2-oxoethyl)-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline 5(4H)-carboxylate
CAS No.:1620090-16-5
Molecular Formula:C₂₄H₂₆N₂O₆S
Molecular Weight:470.546
Hs Code.:

Synonyms:ethyl-4-(2-methoxy-2-oxoethyl)-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline 5(4H)-carboxylate

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Chemical Property of ethyl-4-(2-methoxy-2-oxoethyl)-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline 5(4H)-carboxylate

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Technology Process of ethyl-4-(2-methoxy-2-oxoethyl)-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline 5(4H)-carboxylate

There total 8 articles about ethyl-4-(2-methoxy-2-oxoethyl)-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline 5(4H)-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1620090-27-8
(E)-methyl-3-(2-(2-(ethoxycarbonylamino)phenyl)-1-tosyl-4,5-dihydro-1H-pyrrol-3-yl)acrylate

: 1620090-16-5
ethyl-4-(2-methoxy-2-oxoethyl)-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline 5(4H)-carboxylate

Guidance literature:: With 1-methyl-pyrrolidin-2-one; potassium hydroxide; at 120 ℃; for 12h; Reagent/catalyst; Solvent; Temperature; Time; Inert atmosphere;
DOI:10.1039/c4cc02466d

Reference yield: 58.0%

: 1620090-26-7
ethyl 2-(4-(4-methylphenylsulfonamido)but-1-ynyl)phenylcarbamate

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 1620090-27-8
(E)-methyl-3-(2-(2-(ethoxycarbonylamino)phenyl)-1-tosyl-4,5-dihydro-1H-pyrrol-3-yl)acrylate

: 1620090-16-5
ethyl-4-(2-methoxy-2-oxoethyl)-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline 5(4H)-carboxylate

Guidance literature:: With copper dichloride; palladium dichloride; In N,N-dimethyl-formamide; at 120 ℃; for 18h; Concentration; Solvent; Reagent/catalyst; Temperature; Time; Inert atmosphere;
DOI:10.1039/c4cc02466d

Reference yield:

: 1620090-26-7
ethyl 2-(4-(4-methylphenylsulfonamido)but-1-ynyl)phenylcarbamate

: 1620090-16-5
ethyl-4-(2-methoxy-2-oxoethyl)-1-tosyl-2,3-dihydro-1H-pyrrolo[3,2-c]quinoline 5(4H)-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium dichloride; copper dichloride / toluene / 18 h / 110 °C / Inert atmosphere

2: 1-methyl-pyrrolidin-2-one; potassium hydroxide / 12 h / 120 °C / Inert atmosphere

With 1-methyl-pyrrolidin-2-one; potassium hydroxide; copper dichloride; palladium dichloride; In toluene; 2: |Michael Addition;
DOI:10.1039/c4cc02466d