Technology Process of C2HF3O2*C10H14N4O5
There total 1 articles about C2HF3O2*C10H14N4O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
for 24h;
DOI:10.1002/asia.201100647
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 24 h / 0 - 20 °C
2.1: chlorotriisopropylsilane; trifluoroacetic acid / dichloromethane / 2 h
3.1: 4-methyl-morpholine; triethylamine / dichloromethane / 4 h / 0 °C
4.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 1 h / 0 °C
4.2: 42 h / 0 - 20 °C
5.1: methyl-phenyl-thioether / dichloromethane / 6 h / 0 °C
With
4-methyl-morpholine; chlorotriisopropylsilane; methyl-phenyl-thioether; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid;
In
dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/asia.201100647
