2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene

Base Information

Chemical Name:2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene
CAS No.:159108-85-7
Molecular Formula:C₃₇H₄₈O₈S
Molecular Weight:652.849
Hs Code.:

2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene

Synonyms:2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene

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Chemical Property of 2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene

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Technology Process of 2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene

There total 11 articles about 2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 159108-83-5
2-<2-<(methoxycarbonyl)oxy>-3-methylbut-3-enyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene

: 159108-84-6
(3E,7E)-methyl 2-benzenesulfonyl-4,8,12-trimethyltrideca-3,7,11-trienoate

: 159108-85-7
2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; for 6h; Ambient temperature;
DOI:10.1055/s-1994-25555

Reference yield:

: 24163-93-7,24163-94-8,56881-57-3,6874-67-5,28290-41-7
farnesyl bromide

: 159108-85-7
2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 80 percent / dimethylformamide / 20 °C

2: 90 percent / t-BuOK / -5 - 0 °C

3: 90 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide;

Reference yield:

: 106-28-5
Farnesol

: 159108-85-7
2-<(2E,6E,10E)-5-(benzenesulfonyl)-5-(methoxycarbonyl)-3,7,11,15-tetramethylhexadeca-2,6,10,14-tetraenyl>-1-<(methoxycarbonyl)oxy>-4-methoxybenzene

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / PBr₃ / diethyl ether / -20 °C

2: 80 percent / dimethylformamide / 20 °C

3: 90 percent / t-BuOK / -5 - 0 °C

4: 90 percent / Pd(PPh₃)4 / tetrahydrofuran / 25 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium tert-butylate; phosphorus tribromide; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;