ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-(pentylamino)thiophene-3-carboxylate

Base Information

Chemical Name:ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-(pentylamino)thiophene-3-carboxylate
CAS No.:1334931-35-9
Molecular Formula:C₂₅H₂₇Cl₂NO₃S
Molecular Weight:492.466
Hs Code.:

Synonyms:ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-(pentylamino)thiophene-3-carboxylate

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Chemical Property of ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-(pentylamino)thiophene-3-carboxylate

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Technology Process of ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-(pentylamino)thiophene-3-carboxylate

There total 5 articles about ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-(pentylamino)thiophene-3-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 18.0%

: 1334930-94-7
ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-aminothiophene-3-carboxylate

: 1334931-35-9
ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-(pentylamino)thiophene-3-carboxylate

Guidance literature:: With potassium carbonate; potassium iodide; In N,N-dimethyl-formamide; at 20 - 60 ℃; for 24.5h;
DOI:10.1016/j.ejmech.2011.05.018

Reference yield:

: 1334930-83-4
2-(4-(2,6-dichlorobenzyloxy)phenyl)ethanol

: 1334931-35-9
ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-(pentylamino)thiophene-3-carboxylate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium bromite trihydrate; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium hydrogencarbonate / dichloromethane; water / 0.5 h / 0 - 20 °C / pH 8.6

2: sulfur; triethylamine / ethanol / 60 °C

3: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 24.5 h / 20 - 60 °C

With 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; sodium bromite trihydrate; sodium hydrogencarbonate; potassium carbonate; sulfur; triethylamine; potassium iodide; In ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.05.018

Reference yield:

: 1334930-88-9
2-(4-(2,6-dichlorobenzyloxy)phenyl)acetaldehyde

: 1334931-35-9
ethyl 5-(4-(2,6-dichlorobenzyloxy)phenyl)-2-(pentylamino)thiophene-3-carboxylate

Guidance literature:: Multi-step reaction with 2 steps

1: sulfur; triethylamine / ethanol / 60 °C

2: potassium carbonate; potassium iodide / N,N-dimethyl-formamide / 24.5 h / 20 - 60 °C

With potassium carbonate; sulfur; triethylamine; potassium iodide; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.05.018