O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride

Base Information

• Chemical Name: O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride
• CAS No.: 145149-77-5
• Molecular Formula: C₅₆H₅₉ClO₁₁
• Molecular Weight: 943.531

Synonyms:O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride

Chemical Property of O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride

Chemical Property:

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Technology Process of O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride

There total 1 articles about O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α,β-D-glucopyranose (145149-86-6,145149-87-7) → O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride (145149-77-5)

Guidance literature:

With hydrogenchloride; In diethyl ether; for 48h; Ambient temperature;

DOI:10.1016/S0008-6215(00)90923-6

Reference yield: 83.0%

Methyl 2,4-di-O-benzyl-3-deoxy-α-D-ribo-hexopyranoside (145149-83-3) + O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride (145149-77-5) → Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,4-di-O-benzyl-3-deoxy-α-D-ribo-hexopyranoside (145149-89-9)

Guidance literature:

With 2,4,6-trimethyl-pyridine; silver perchlorate; In diethyl ether; at -30 ℃;

DOI:10.1016/S0008-6215(00)90923-6

Reference yield: 78.0%

Methyl 3,4-di-O-benzyl-2-deoxy-α-D-arabino-hexopyranoside (145149-85-5) + O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3,4-tri-O-benzyl-α-D-glucopyranosyl chloride (145149-77-5) → Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-3,4-di-O-benzyl-2-deoxy-α-D-arabino-hexopyranoside

Guidance literature:

With 2,4,6-trimethyl-pyridine; silver perchlorate; In diethyl ether; at -30 ℃;

DOI:10.1016/S0008-6215(00)90923-6

upstream raw materials:

O-(6-O-Acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-1-O-acetyl-2,3,4-tri-O-benzyl-α,β-D-glucopyranose

Downstream raw materials:

Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,4-di-O-benzyl-3-deoxy-α-D-ribo-hexopyranoside

Methyl O-(6-O-acetyl-2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-deoxy-α-D-xylo-hexopyranoside

Methyl O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-O-(2,3,4-tri-O-benzyl-α-D-glucopyranosyl)-(1->6)-4-deoxy-α-D-xylo-hexopyranoside

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