ethyl (2E)-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[[N-(4-methylphenyl)sulfonyl][2-[(phenylmethoxyimino)methyl]phenyl]amino]-2-heptenoate

Base Information

• Chemical Name: ethyl (2E)-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[[N-(4-methylphenyl)sulfonyl][2-[(phenylmethoxyimino)methyl]phenyl]amino]-2-heptenoate
• CAS No.: 1032651-65-2
• Molecular Formula: C₃₆H₄₈N₂O₆SSi
• Molecular Weight: 664.938

Synonyms:ethyl (2E)-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[[N-(4-methylphenyl)sulfonyl][2-[(phenylmethoxyimino)methyl]phenyl]amino]-2-heptenoate

Chemical Property of ethyl (2E)-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[[N-(4-methylphenyl)sulfonyl][2-[(phenylmethoxyimino)methyl]phenyl]amino]-2-heptenoate

Chemical Property:

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Technology Process of ethyl (2E)-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[[N-(4-methylphenyl)sulfonyl][2-[(phenylmethoxyimino)methyl]phenyl]amino]-2-heptenoate

There total 1 articles about ethyl (2E)-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[[N-(4-methylphenyl)sulfonyl][2-[(phenylmethoxyimino)methyl]phenyl]amino]-2-heptenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

ethyl (E)-4-hydroxy-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-heptenoate (1032651-68-5) + N-[2-(benzyloxyimino-methyl)-phenyl]-4-methyl-benzenesulfonamide (705256-10-6) → ethyl (2E)-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[[N-(4-methylphenyl)sulfonyl][2-[(phenylmethoxyimino)methyl]phenyl]amino]-2-heptenoate (1032651-65-2)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; toluene; at 20 ℃;

DOI:10.1021/jo800560p

Reference yield: 30.0%

ethyl (2E)-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-4-[[N-(4-methylphenyl)sulfonyl][2-[(phenylmethoxyimino)methyl]phenyl]amino]-2-heptenoate (1032651-65-2) → (3aβ,4β,9bβ)-1,3,3a,4,5,9b-hexahydro-4-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-5-[(4-methylphenyl)sulfonyl]-2H-pyrrolo[3,2-c]quinolin-2-one + (3aα,4β,9bβ)-1,3,3a,4,5,9b-hexahydro-4-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-5-[(4-methylphenyl)sulfonyl]-2H-pyrrolo[3,2-c]quinolin-2-one + (3aβ,4α,9bβ)-1,3,3a,4,5,9b-hexahydro-4-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-5-[(4-methylphenyl)sulfonyl]-2H-pyrrolo[3,2-c]quinolin-2-one + ethyl (2α,3β,4α)-1,2,3,4-tetrahydro-2-[3-[[(1,1-dimethylethyl)dimethylsilyl]oxy]propyl]-1-[(4-methylphenyl)sulfonyl]-4-[(phenylmethoxy)amino]quinolin-3-acetate

Guidance literature:

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In benzene; for 4.5h; Heating;

DOI:10.1021/jo800560p

upstream raw materials:

ethyl (E)-4-hydroxy-7-[[(1,1-dimethylethyl)dimethylsilyl]oxy]-2-heptenoate

N-[2-(benzyloxyimino-methyl)-phenyl]-4-methyl-benzenesulfonamide

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