trans-hydridoamminebis(tricyclohexylphosphine)platinum perchlorate

Base Information

Chemical Name:trans-hydridoamminebis(tricyclohexylphosphine)platinum perchlorate
CAS No.:110719-80-7
Molecular Formula:C₃₆H₇₀NP₂Pt*ClO₄
Molecular Weight:873.437
Hs Code.:

Synonyms:trans-hydridoamminebis(tricyclohexylphosphine)platinum perchlorate

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Chemical Property of trans-hydridoamminebis(tricyclohexylphosphine)platinum perchlorate

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Technology Process of trans-hydridoamminebis(tricyclohexylphosphine)platinum perchlorate

There total 1 articles about trans-hydridoamminebis(tricyclohexylphosphine)platinum perchlorate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 42764-88-5
trans-chlorohydridobis(tricyclohexylphosphine)platinum(II)

: silver perchlorate

: 110719-80-7
trans-hydridoamminebis(tricyclohexylphosphine)platinum perchlorate

Guidance literature:: With NH₃; In methanol; chloroform; byproducts: AgCl; (N2); added dropwise a soln. of AgClO4 in methanol to a stirred soln. of Pt-complex; stirred for 30 min; filtered; bubbled NH3 through the soln. for 1 min; added n-hexane; dissolved in CH2Cl2; added diethyl ether; pptd.; recrystd. by addn. of diethyl ether to a CH2Cl2 soln.; elem. anal.;
DOI:10.1021/om00049a020

Reference yield:

: 110719-80-7
trans-hydridoamminebis(tricyclohexylphosphine)platinum perchlorate

: 110719-81-8
trans-hydridoamidobis(tricyclohexylphosphine)platinum

Guidance literature:: With NaNH₂; In benzene-d6; ammonia; byproducts: NH3, NaClO4; NH3 (liquid); (N2); stirred for 1 h;
DOI:10.1021/om00049a020

Reference yield:

: 110719-80-7
trans-hydridoamminebis(tricyclohexylphosphine)platinum perchlorate

: 42764-88-5
trans-chlorohydridobis(tricyclohexylphosphine)platinum(II)

Guidance literature:: Multi-step reaction with 2 steps

1: NaNH₂ / benzene-d6; ammonia

2: not given

With NaNH₂; In benzene-d6; ammonia;
DOI:10.1021/om00049a020