9,9-diethoxy-1,7-diphenyl-8,10-dioxa-3,4,5-trithia-9-siladodecyl triethyl orthosilicate

Base Information

Chemical Name:9,9-diethoxy-1,7-diphenyl-8,10-dioxa-3,4,5-trithia-9-siladodecyl triethyl orthosilicate
CAS No.:1278475-69-6
Molecular Formula:C₂₈H₄₆O₈S₃Si₂
Molecular Weight:663.037
Hs Code.:

Synonyms:9,9-diethoxy-1,7-diphenyl-8,10-dioxa-3,4,5-trithia-9-siladodecyl triethyl orthosilicate

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Chemical Property of 9,9-diethoxy-1,7-diphenyl-8,10-dioxa-3,4,5-trithia-9-siladodecyl triethyl orthosilicate

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Technology Process of 9,9-diethoxy-1,7-diphenyl-8,10-dioxa-3,4,5-trithia-9-siladodecyl triethyl orthosilicate

There total 2 articles about 9,9-diethoxy-1,7-diphenyl-8,10-dioxa-3,4,5-trithia-9-siladodecyl triethyl orthosilicate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 78-10-4
tetraethoxy orthosilicate

: 1278475-40-3
2-[3-(2-hydroxy-2-phenylethyl)trisulfanyl]-1-phenyl-1-ethanol

: 1278475-69-6
9,9-diethoxy-1,7-diphenyl-8,10-dioxa-3,4,5-trithia-9-siladodecyl triethyl orthosilicate

Guidance literature:: tetraethoxy orthosilicate; 2-[3-(2-hydroxy-2-phenylethyl)trisulfanyl]-1-phenyl-1-ethanol; With trifluoroacetic acid; In 1,2-dimethoxyethane; at 60 ℃; for 24h;

With potassium carbonate; In 1,2-dimethoxyethane; at 20 ℃; for 1h;
DOI:10.1016/j.electacta.2010.11.064

Reference yield:

: 96-09-3
styrene oxide

: 1278475-69-6
9,9-diethoxy-1,7-diphenyl-8,10-dioxa-3,4,5-trithia-9-siladodecyl triethyl orthosilicate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / ethanol; water / 15.5 h / 20 - 25 °C

2.1: trifluoroacetic acid / 1,2-dimethoxyethane / 24 h / 60 °C

2.2: 1 h / 20 °C

With sodium hydrogencarbonate; trifluoroacetic acid; In 1,2-dimethoxyethane; ethanol; water;
DOI:10.1016/j.electacta.2010.11.064