C₄₃H₅₀N₈O₁₀S₂

Base Information

Chemical Name:C₄₃H₅₀N₈O₁₀S₂
CAS No.:1399362-68-5
Molecular Formula:C₄₃H₅₀N₈O₁₀S₂
Molecular Weight:903.05
Hs Code.:

C<sub>43</sub>H<sub>50</sub>N<sub>8</sub>O<sub>10</sub>S<sub>2</sub>

Synonyms:C₄₃H₅₀N₈O₁₀S₂

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Chemical Property of C₄₃H₅₀N₈O₁₀S₂

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Technology Process of C₄₃H₅₀N₈O₁₀S₂

There total 23 articles about C₄₃H₅₀N₈O₁₀S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1391396-76-1
C₄₄H₅₂N₈O₁₀S₂

: 1399362-68-5
C₄₃H₅₀N₈O₁₀S₂

Guidance literature:: C₄₄H₅₂N₈O₁₀S₂; With lithium hydroxide; In methanol; dichloromethane; at 20 ℃; for 8h;

In methanol; dichloromethane; water; pH=1; Acidic conditions;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: 1064764-00-6
methyl 2-(2-methyl-2-tert-butoxy-1-tert-butoxycarbonylamino-ethyl)-oxazole-4-carboxylate

: 1399362-68-5
C₄₃H₅₀N₈O₁₀S₂

Guidance literature:: Multi-step reaction with 15 steps

1.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

1.2: pH 1 / Acidic conditions

2.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

3.1: palladium 10% on activated carbon; hydrogen / ethanol

4.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

5.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

6.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

6.2: 12 h / -20 - 20 °C / Inert atmosphere

7.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

8.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

9.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

9.2: 3 h / 0 °C / Inert atmosphere

9.3: 3 h / 20 °C / Inert atmosphere

10.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

11.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

12.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

12.2: 3 h / 0 °C / Inert atmosphere

12.3: 3 h / 20 °C / Inert atmosphere

13.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

13.2: pH 1 / Acidic conditions

14.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

15.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

15.2: pH 1 / Acidic conditions

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 9.1: Hantzsch thiazole synthesis / 9.2: Hantzsch thiazole synthesis / 9.3: Hantzsch thiazole synthesis / 12.1: Hantzsch thiazole synthesis / 12.2: Hantzsch thiazole synthesis / 12.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105

Reference yield:

: 1391396-36-3
C₂₇H₃₉N₃O₈

: 1399362-68-5
C₄₃H₅₀N₈O₁₀S₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: palladium 10% on activated carbon; hydrogen / ethanol

2.1: diethylamino-sulfur trifluoride / dichloromethane / 1 h / -78 °C / Inert atmosphere

3.1: potassium carbonate / dichloromethane / -78 - 20 °C / Inert atmosphere

4.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / dichloromethane / 0.25 h / -20 °C / Inert atmosphere

4.2: 12 h / -20 - 20 °C / Inert atmosphere

5.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

6.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

7.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

7.2: 3 h / 0 °C / Inert atmosphere

7.3: 3 h / 20 °C / Inert atmosphere

8.1: ammonium hydroxide / methanol; water / 20 °C / Sonication

9.1: Lawessons reagent / 1,2-dimethoxyethane / 60 °C / Inert atmosphere

10.1: potassium hydrogencarbonate / 1,2-dimethoxyethane / 16 h / 20 °C / Inert atmosphere

10.2: 3 h / 0 °C / Inert atmosphere

10.3: 3 h / 20 °C / Inert atmosphere

11.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

11.2: pH 1 / Acidic conditions

12.1: O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.75 h / 20 °C / Inert atmosphere

13.1: lithium hydroxide / methanol; dichloromethane / 8 h / 20 °C

13.2: pH 1 / Acidic conditions

With Lawessons reagent; ammonium hydroxide; diethylamino-sulfur trifluoride; palladium 10% on activated carbon; hydrogen; potassium carbonate; potassium hydrogencarbonate; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; lithium hydroxide; In methanol; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 7.1: Hantzsch thiazole synthesis / 7.2: Hantzsch thiazole synthesis / 7.3: Hantzsch thiazole synthesis / 10.1: Hantzsch thiazole synthesis / 10.2: Hantzsch thiazole synthesis / 10.3: Hantzsch thiazole synthesis;
DOI:10.1016/j.tetlet.2012.05.105