14-phenyl-9H-benzo[e]phenanthro[1,10-bc]oxepine

Base Information

• Chemical Name: 14-phenyl-9H-benzo[e]phenanthro[1,10-bc]oxepine
• CAS No.: 1384159-73-2
• Molecular Formula: C₂₇H₁₈O
• Molecular Weight: 358.439
• Mol file: 1384159-73-2.mol

Synonyms:14-phenyl-9H-benzo[e]phenanthro[1,10-bc]oxepine

Chemical Property of 14-phenyl-9H-benzo[e]phenanthro[1,10-bc]oxepine

Chemical Property:

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Technology Process of 14-phenyl-9H-benzo[e]phenanthro[1,10-bc]oxepine

There total 1 articles about 14-phenyl-9H-benzo[e]phenanthro[1,10-bc]oxepine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

1-iodo-2-((2-(phenylethynyl)benzyl)oxy)benzene (1384159-84-5) + 2-(trimethylsilyl)phenyl trifluoromethanesulfonate (88284-48-4) → 14-phenyl-9H-benzo[e]phenanthro[1,10-bc]oxepine (1384159-73-2)

Guidance literature:

With thallium(I) acetate; cesium fluoride; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; acetonitrile; at 85 ℃; for 8h; Inert atmosphere;

DOI:10.1039/c2cc31807e

upstream raw materials:

1-iodo-2-((2-(phenylethynyl)benzyl)oxy)benzene

2-(trimethylsilyl)phenyl trifluoromethanesulfonate