acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside

Base Information

Chemical Name:acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside
CAS No.:325474-97-3
Molecular Formula:C₁₆H₂₀O₈S
Molecular Weight:372.396
Hs Code.:

Synonyms:acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside

Suppliers and Price of acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside

There total 3 articles about acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 108-24-7
acetic anhydride

: 325474-95-1
4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranose

: 325474-97-3
acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside

Guidance literature:: With pyridine; at 0 ℃; for 14h;
DOI:10.1016/S0040-4020(00)00868-1

Reference yield:

: 72062-67-0
Benzoic acid (2S,3R,4S,6S)-2-bromomethyl-4-methanesulfonyloxy-6-methoxy-tetrahydro-pyran-3-yl ester

: 325474-97-3
acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside

Guidance literature:: Multi-step reaction with 3 steps

1: 96 percent / H₂; Et₃N / Raney nickel / methanol; H₂O / 12 h / 20 °C

2: 84 percent / aq. HOAc; aq. HCl / 1.5 h / Heating

3: 87 percent / pyridine / 14 h / 0 °C

With pyridine; hydrogenchloride; hydrogen; acetic acid; triethylamine; nickel; In methanol; water;
DOI:10.1016/S0040-4020(00)00868-1

Reference yield:

: 72062-68-1
methyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranoside

: 325474-97-3
acetyl 4-O-benzoyl-3-O-methanesulfonyl-2,6-dideoxy-α-D-ribo-hexopyranosside

Guidance literature:: Multi-step reaction with 2 steps

1: 84 percent / aq. HOAc; aq. HCl / 1.5 h / Heating

2: 87 percent / pyridine / 14 h / 0 °C

With pyridine; hydrogenchloride; acetic acid;
DOI:10.1016/S0040-4020(00)00868-1