1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline

Base Information

Chemical Name:1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline
CAS No.:142683-49-6
Molecular Formula:C₂₇H₂₆N₂O₄
Molecular Weight:442.514
Hs Code.:

Synonyms:1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline

Suppliers and Price of 1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

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Hazard Codes:

MSDS Files:

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Technology Process of 1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline

There total 3 articles about 1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 142683-35-0
methyl N-(diphenylmethylene)-5,6-dimethoxytryptophanate

: 142683-49-6
1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 10h; Heating;
DOI:10.1002/jhet.5570290205

Reference yield:

: 118553-21-2
Methyl N-(diphenylmethylene)-α,β-didehydroalaninate

: 142683-49-6
1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / ethylaluminum dichloride / CH₂Cl₂; hexane / 1 h / 0 °C

2: 65 percent / p-toluenesulfonic acid / toluene / 10 h / Heating

With ethylaluminum dichloride; toluene-4-sulfonic acid; In hexane; dichloromethane; toluene;
DOI:10.1002/jhet.5570290205

Reference yield:

: 14430-23-0
5,6-dimethoxyindole

: 142683-49-6
1,1-diphenyl-3-carbomethoxy-6,7-dimethoxy-1,2,3,4-tetrahydro-β-carboline

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / ethylaluminum dichloride / CH₂Cl₂; hexane / 1 h / 0 °C

2: 65 percent / p-toluenesulfonic acid / toluene / 10 h / Heating

With ethylaluminum dichloride; toluene-4-sulfonic acid; In hexane; dichloromethane; toluene;
DOI:10.1002/jhet.5570290205