2-{[3-cyano-4-(4-methoxyphenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-2-yl]sulfanyl}-N-(4-methylphenyl)acetamide

Base Information

Chemical Name:2-{[3-cyano-4-(4-methoxyphenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-2-yl]sulfanyl}-N-(4-methylphenyl)acetamide
CAS No.:345912-30-3
Molecular Formula:C₂₅H₂₃N₃O₂S
Molecular Weight:429.543
Hs Code.:
Mol file:345912-30-3.mol

Synonyms:2-[3-cyano-4-(4-methoxy-phenyl)-6,7-dihydro-5H-[1]pyrindin-2-ylsulfanyl]-N-p-tolyl-acetamide

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Chemical Property of 2-{[3-cyano-4-(4-methoxyphenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-2-yl]sulfanyl}-N-(4-methylphenyl)acetamide

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Technology Process of 2-{[3-cyano-4-(4-methoxyphenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-2-yl]sulfanyl}-N-(4-methylphenyl)acetamide

There total 1 articles about 2-{[3-cyano-4-(4-methoxyphenyl)-6,7-dihydro-5H-cyclopenta[b]pyridin-2-yl]sulfanyl}-N-(4-methylphenyl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 16634-82-5
N-(p-tolyl)-2-chloroacetamide

: 120517-49-9
4-(4-methoxyphenyl)-2-sulfanylidene-1H,2H,5H,6H,7H-cyclopenta[b]pyridine-3-carbonitrile

: 345912-30-3
2-[3-cyano-4-(4-methoxy-phenyl)-6,7-dihydro-5H-[1]pyrindin-2-ylsulfanyl]-N-p-tolyl-acetamide

Guidance literature:: With sodium acetate; In ethanol; for 2h; Heating;
DOI:10.1080/10426500008076538

Reference yield: 90.0%

: 345912-30-3
2-[3-cyano-4-(4-methoxy-phenyl)-6,7-dihydro-5H-[1]pyrindin-2-ylsulfanyl]-N-p-tolyl-acetamide

: 345912-42-7
3-amino-4-(4-methoxy-phenyl)-6,7-dihydro-5H-1-thia-8-aza-s-indacene-2-carboxylic acid p-tolylamide

Guidance literature:: With sodium ethanolate; In ethanol; for 0.0833333h; Heating;
DOI:10.1080/10426500008076538

Reference yield:

: 345912-30-3
2-[3-cyano-4-(4-methoxy-phenyl)-6,7-dihydro-5H-[1]pyrindin-2-ylsulfanyl]-N-p-tolyl-acetamide

: 345912-81-4
4-(4-methoxy-phenyl)-7-p-tolyl-2,3-dihydro-1H,7H-9-thia-5,6,7,10-tetraaza-cyclopenta[b]fluoren-8-one

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / EtONa / ethanol / 0.08 h / Heating

2: 77 percent / NaNO₂; AcOH; H₂SO₄ / 0 °C

With sulfuric acid; sodium ethanolate; acetic acid; sodium nitrite; In ethanol; 1: Thorpe-Ziegler cyclization;
DOI:10.1080/10426500008076538