C₃₇H₆₇N₃O₅Si₂

Base Information

Chemical Name:C₃₇H₆₇N₃O₅Si₂
CAS No.:922523-38-4
Molecular Formula:C₃₇H₆₇N₃O₅Si₂
Molecular Weight:690.127
Hs Code.:

C<sub>37</sub>H<sub>67</sub>N<sub>3</sub>O<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₇H₆₇N₃O₅Si₂

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Chemical Property of C₃₇H₆₇N₃O₅Si₂

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Technology Process of C₃₇H₆₇N₃O₅Si₂

There total 15 articles about C₃₇H₆₇N₃O₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 896729-89-8
(3S,5R)-6-azido-3,5-dimethylhexan-2-one

: 922523-37-3
C₂₉H₅₂O₄Si₂

: 922523-38-4
C₃₇H₆₇N₃O₅Si₂

Guidance literature:: With lithium diisopropyl amide; In tetrahydrofuran; hexane; for 0.25h; cooling;
DOI:10.1002/anie.200603353

Reference yield:

: 922523-52-2
C₂₅H₃₅NO₄S

: 922523-38-4
C₃₇H₆₇N₃O₅Si₂

Guidance literature:: Multi-step reaction with 9 steps

1.1: 89 percent / DIBAL-H / CH₂Cl₂ / 2 h

2.1: Et₃N; (cyclohexyl)2BOTf / CH₂Cl₂; hexane / 2.33 h

2.2: 86 percent / CH₂Cl₂ / 14 h / cooling

3.1: 17.1 mmol / NaH / various solvent(s) / 0.42 h

4.1: 75 percent / 2,6-lutidine / CH₂Cl₂ / 0.58 h

5.1: 98 percent / ceric ammonium nitrate / acetonitrile; H₂O / 1 h

6.1: 86 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h

7.1: 59 percent / diisobutylaluminium hydride / CH₂Cl₂ / -78 - 20 °C

8.1: 80 percent / Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 1 h / 20 °C

9.1: 94 percent / LDA / hexane; tetrahydrofuran / 0.25 h / cooling

With 2,6-dimethylpyridine; ammonium cerium(IV) nitrate; sodium hydride; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; triethylamine; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.200603353

Reference yield:

: 922523-31-7
C₃₄H₄₂O₈

: 922523-38-4
C₃₇H₆₇N₃O₅Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: 75 percent / 2,6-lutidine / CH₂Cl₂ / 0.58 h

2: 98 percent / ceric ammonium nitrate / acetonitrile; H₂O / 1 h

3: 86 percent / 2,6-lutidine / CH₂Cl₂ / 0.5 h

4: 59 percent / diisobutylaluminium hydride / CH₂Cl₂ / -78 - 20 °C

5: 80 percent / Dess-Martin periodinane; NaHCO₃ / CH₂Cl₂ / 1 h / 20 °C

6: 94 percent / LDA / hexane; tetrahydrofuran / 0.25 h / cooling

With 2,6-dimethylpyridine; ammonium cerium(IV) nitrate; diisobutylaluminium hydride; sodium hydrogencarbonate; Dess-Martin periodane; lithium diisopropyl amide; In tetrahydrofuran; hexane; dichloromethane; water; acetonitrile;
DOI:10.1002/anie.200603353