4-(benzyloxy)-N-(3'-(benzyloxy)propan-2'-one)-1-bromo-N-tosyl-3-naphthylamine

Base Information

Chemical Name:4-(benzyloxy)-N-(3'-(benzyloxy)propan-2'-one)-1-bromo-N-tosyl-3-naphthylamine
CAS No.:144318-41-2
Molecular Formula:C₃₄H₃₀BrNO₅S
Molecular Weight:644.586
Hs Code.:

Synonyms:4-(benzyloxy)-N-(3'-(benzyloxy)propan-2'-one)-1-bromo-N-tosyl-3-naphthylamine

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Chemical Property of 4-(benzyloxy)-N-(3'-(benzyloxy)propan-2'-one)-1-bromo-N-tosyl-3-naphthylamine

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Technology Process of 4-(benzyloxy)-N-(3'-(benzyloxy)propan-2'-one)-1-bromo-N-tosyl-3-naphthylamine

There total 8 articles about 4-(benzyloxy)-N-(3'-(benzyloxy)propan-2'-one)-1-bromo-N-tosyl-3-naphthylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 122745-35-1
3-Amino-1-(benzyloxy)naphthalene

: 144318-41-2
4-(benzyloxy)-N-(3'-(benzyloxy)propan-2'-one)-1-bromo-N-tosyl-3-naphthylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine / 48 h / 25 °C

2: 92 percent / N-bromosuccinimide, H₂SO₄ / tetrahydrofuran / 8.5 h / -78 °C

3: 1.) NaH / 1.) DMF, 23 deg C, 2 h, 2.) DMF, a) 0 deg C, 24 h, b) 25 deg C, 24 h

With pyridine; N-Bromosuccinimide; sulfuric acid; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja00050a012

Reference yield:

: 144318-39-8
1-(benzyloxy)-N-tosyl-3-naphthylamine

: 144318-41-2
4-(benzyloxy)-N-(3'-(benzyloxy)propan-2'-one)-1-bromo-N-tosyl-3-naphthylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / N-bromosuccinimide, H₂SO₄ / tetrahydrofuran / 8.5 h / -78 °C

2: 1.) NaH / 1.) DMF, 23 deg C, 2 h, 2.) DMF, a) 0 deg C, 24 h, b) 25 deg C, 24 h

With N-Bromosuccinimide; sulfuric acid; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja00050a012

Reference yield:

: 98-59-9
p-toluenesulfonyl chloride

: 144318-41-2
4-(benzyloxy)-N-(3'-(benzyloxy)propan-2'-one)-1-bromo-N-tosyl-3-naphthylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / pyridine / 48 h / 25 °C

2: 92 percent / N-bromosuccinimide, H₂SO₄ / tetrahydrofuran / 8.5 h / -78 °C

3: 1.) NaH / 1.) DMF, 23 deg C, 2 h, 2.) DMF, a) 0 deg C, 24 h, b) 25 deg C, 24 h

With pyridine; N-Bromosuccinimide; sulfuric acid; sodium hydride; In tetrahydrofuran;
DOI:10.1021/ja00050a012